SSW_S2013_02

Solid State Welding Spring 2013 Session · 9 sections 27 cases · Watch on YouTube ↗ all files
Layer 3 — readable edition

§1. Welding as an interdisciplinary, ubiquitous, failure-prone field [00:06]

§1.p1

Studying welding and joining is integrative. It uses lots of interdisciplinary fields. It's not just a materials field — it's physics, chemistry, structures, civil engineering, mechanical engineering, electrical engineering, chemical engineering. It's a whole bunch of things. Welding is about 150 years old in terms of electric arc welding. It goes back thousands of years to people using forges and soldering and things like that.

§1.p2

It's ubiquitous. Very few manufactured products don't contain a joint. In fact, any product that uses two dissimilar materials has to have a joint between them. To have no joint, you have to have a monolithic material that's a standalone product useful in its own right rather than just a paperweight, and it's usually something fairly large. For years I got pieces like needles and things brought in. One student came up with a cast iron frying pan. Professor McClintock came up with an anvil. Has anyone come up with anything any larger? It turns out Professor Pelloux heard this once and he came up with an anvil — but it was the anvil of a forging press, about a thousand tons. So he may win the prize for the largest standalone object. It was a huge casting.

§1.p3

There are many failures, and this is kind of where we stopped last time. When I heard about the Space Shuttle Challenger in 1986 — my students told me about it that morning — I said, "I bet it failed at a weld." I was wrong, but it did fail at an O-ring joint. It was at a joint. Things typically fail at joints because they're the highest-stress locations in the structure. It's just sort of natural. They also may not be 100% efficient depending on the material.

§2. The Alexander Kielland: a non-critical weld brings down a platform [02:30]

§2.p1

There are some huge failures that cost a billion dollars or take lots of lives. There's an offshore oil platform called the Alexander Kielland, about 1980 in the North Sea. This was supposed to be a production platform for oil in the North Sea, and they changed it to a hotel. A great big storm comes by — these things should have been safe in a storm — but the whole thing capsized, and over 200 people died.

§2.p2

When they did the analysis, they found that the French shipyard that had built this offshore oil platform — someone had taken about a 16-inch diameter piece of steel and welded it to one of these legs. One of these legs on an offshore oil platform is a big piece of round steel about the diameter of this room. They had welded this 16-inch-diameter, basketball-sized piece on because they were going to put a sonar instrument there.

§2.p3

No one thought this was a critical part of the structure. The management of the shipyard had one group of people who worried about welding steel that went into the main structure — the great big 24-foot-diameter legs. They let the maintenance people worry about welding hanger-on pieces like this sonar bracket. The maintenance people went to the shop and got a pipe. It turns out it was a high-carbon steel pipe, and if you weld high-carbon steel, it's very easy to get cracking. They had a little crack about the size of your thumbnail. No one found it, because it wasn't a critical part of the structure — all the inspection was for the critical parts, like the welds in those 24-foot-diameter legs. The waves came along, and over time a fatigue crack grew to where it was 20-some feet long. When the storm came by, this 20-foot-long crack just snapped it. That's what caused the accident.

§2.p4

There are a lot of other things people said caused the accident. If you look up the Alexander Kielland, you'll find all kinds of stories — a lot of people said the cause was that they didn't have enough lifeboats. Well, you didn't need lifeboats if the structure hadn't failed. So it's a question of where you start your accounting.

§3. Steel dominates; welding is applied as an art [05:18]

§3.p1

I handed out a paper on the future of metals and pointed out that iron and steel constitute 95 pounds out of every 100 pounds of metal made in the world. Aluminum is less than 2%. Iron and steel is about a billion tons a year, so aluminum at 2% is about 20 million tons a year. That's a lot of aluminum, but it's nothing compared to the amount of steel. In fusion welding we'll talk a lot more about iron and steel because it's the dominant material, and in material selection you'll hear about why.

§3.p2

Welding is often applied as an art. As soon as someone gets a new heat source, they often try to use it to weld. People discovered over the ages how to do soldering and brazing on art objects. They even learned to do diffusion bonding. When we get to diffusion bonding, I'll tell you the story about how the Etruscans used to use tin to bond gold beads to copper objects. They just put them in a furnace and ended up getting a type of diffusion bond. I always say Pratt & Whitney patented this process in 1972 only because the Etruscans, who used it in 600 BC, didn't file an infringement against them. Some people think that King Tut's dagger had the same type of gold beads attached to it by this type of diffusion bonding. No one knows because no one's willing to cut up the dagger to find out.

§3.p3

Welding was initially used as an art to make all kinds of vessels. If you go to Kyoto, Japan, Sumitomo has a museum of Chinese castings — Sumitomo is a metals company in Japan, and 5,000 years ago the Chinese were making bronze castings. They had to weld on legs and things, and they did it by pouring molten metal between the leg and the other casting to make a more complex product. In the Middle Ages a lot of what was driving joining technology was military needs. Then people started discovering new types of science. Humphry Davy discovered the arc, gave the name to the electric arc in 1805 or 1806, and he tried to weld with it within the next year.

§3.p4

The earliest commercial use of a laser was in the mid-50s. Lasers were only invented in the mid-50s, but it's my understanding that General Electric used to use them this way: back in the mid-50s, people used vacuum tubes in their electronics. We didn't have silicon yet — silicon had been invented as a semiconductor in 1947, but it really hadn't been commercialized. So most power electronics had vacuum tubes, and some of these tubes would cost a couple hundred or $1,000. Back in 1950, that's a lot of money. So they would make these things, seal them in vacuum, and then find out that one of the joints inside had failed. Supposedly General Electric took a research laser — you'd have two tungsten or molybdenum wires inside the clear glass vacuum tube — and they would first hit it with a soft electron laser beam that would just soften the wire so it would make contact with the other wire, then come in with power and weld it back together to make the electrical connection and save the vacuum tube. So lasers were used early on. Electron beams were used early on, within the first five or ten years of their having been developed into high-power devices.

§3.p5

In my own experience, particle beams have been used for welding. In the mid-70s, they were making high-power lasers for military applications, but over here in Everett, Massachusetts — it's now the Mellon Bank building — AVCO Everett Research Laboratories had 25-kilowatt lasers developed for commercial applications under government contracts, and they tried to laser-weld heavy pieces of steel and other materials. One of my students went to work for them, and he said his main job was making sure the laser worked when one of the customers would come in to look at it, because 90% of the time it didn't even work.

§4. Particle beams, the Sheffield, and titanium submarines [10:57]

§4.p1

In the early 90s, the military had spent a quarter billion dollars developing particle-beam weapons — proton beams the Navy was supposedly going to shoot through the air to shoot down a missile coming toward the ship. In the Falkland Islands War in the 80s, a French Exocet missile fired by the Argentinians hit the British cruiser Sheffield, and an aluminum fire started. There's debate on whether it was an aluminum fire, but it probably was, and it wiped out the entire ship. One small missile that you could buy from arms dealers anywhere in the world could wipe out a capital ship of one of the world's major navies. So the US Navy was trying to develop these particle-beam weapons from the mid-80s through the early 90s, and then peace broke out with the former Soviet Union. They weren't quite as concerned anymore, but they had spent a quarter billion dollars and they wanted to find some application. They had a three-day workshop, invited me to it, and said, "Can we use these to weld nuclear submarines?" I went down and said, "Well, maybe you can melt a nuclear submarine, but with 5 megawatts of power, you don't need that to weld. You only need a few tens of kilowatts."

§4.p2

Anyway, I got a research project in the mid-90s to see if we could use particle-beam weapons to do welding and heat treatment. As soon as a new heat source technology comes along, people use it, and they don't necessarily understand it. So welding is often applied as an art, and along with that, relatively few people have been trained in welding. It is an interdisciplinary field. There are materials engineers who, like myself — I went to work for a steel company, and they said, "You're a welding engineer." I had never taken a welding course in my life, but all of a sudden I was a welding engineer. And I met many physicists whose manager would call them in and say, "You're now a welding engineer." They took physics classes. They didn't know anything about welding. And you can kind of see how they kept reinventing the wheel, because they took what they knew from physics and tried to apply it to welding. It doesn't always work. The physics of welding is a little different than what you learn in the classroom.

§4.p3

There are very few people trained in welding in this country. There's one school that gives a four-year degree from a regular university — Ohio State University, which has had a welding engineering department for the last 60 years, though that department is now folded in with a couple of others. Highest-paid students in the School of Engineering at Ohio State. Industry wants them. If you go to the former Soviet Union, they had the Paton Institute in Kiev. For political reasons, the Paton Institute used to get huge amounts of money from the Soviet government. It's an institute of 10,000 people studying welding, though they study a lot of other things too, like casting.

§4.p4

Professor Paton — I think he just passed away a year or two ago — his father had weld-repaired Soviet tanks during World War II and got them back to the front to fight Hitler. He was a hero of the Soviet Union. After the war, under the Stalin regime, the son took over in the 40s and 50s this Paton Welding Institute named after the father. It's kind of fuzzy whether it's named after the father or the son. Professor Paton was head of the Ukrainian Academy of Sciences, and in the former Soviet Union all the research money from the central government came through the Academy of Sciences and was divvied up. There were only seven people on the Soviet Academy of Sciences, and Professor Paton was one of those seven. The Ukraine was the largest and most financially successful of all the provinces in the former Soviet Union, so they got more research money than any other province, because Professor Paton represented Ukraine, and when the money came to the Ukraine, he gave most of it to his institute. Corruption at its best.

§4.p5

So they had a huge welding institute and they developed technologies like — if you've ever read The Hunt for Red October or seen the movie, they had titanium submarines. My first research project, in 1977, was from the US Navy to weld titanium for submarines. [Tom holds up a 1977-era titanium weld sample.] This probably belongs in the Smithsonian. We were welding 1-inch-thick titanium for submarines. The United States wanted to build titanium submarines. We never built one, other than the deep-sea research vessel Alvin that went down and found the Titanic. The Navy built that as part of a prototype program to learn to weld titanium for bigger ships, because titanium submarines have the same strength-to-weight ratio advantage that aircraft and fast-moving vehicles need. You want high strength-to-weight so you can dive deeper and, hopefully, if you lose power, pop to the surface rather than sink to the bottom — because if you sink to the bottom, everything gets crushed, including the people inside.

§4.p6

The Soviets actually built a titanium submarine. [Tom holds up a weld made at Oregon Graduate Center.] This is a weld made at Oregon Graduate Center by one of the processes developed by Dr. Gurevich at the Paton Institute, because the Soviets spent hundreds of millions of dollars. We couldn't justify building the titanium submarine or spending the money to do the research, but the Soviets were under a different economic system and were driven by military needs much more than we are. It turns out their titanium submarine was somewhat of a disaster, and within two or three years they all just parked them in the harbor because they were developing leaks. The US Navy asked me, "How did the Soviets solve the creep-fatigue interaction of the titanium?" Titanium has this problem: if you put it under continuous compressive stress, even at room temperature or seawater temperature, it will start to slowly creep. Then if you flex it, there's an interaction, and the cracks grow ultra-fast. In 1980, when we learned about the Soviet Alfa subs, I went to some workshops and they said, "How'd they solve the problem?" I said, "I don't know." It turns out they didn't. They built these submarines and they had cracks. They had to park them.

§4.p7

But anyway, the US Navy's never built them for various reasons, mostly economic. With the poor training in this country, we produce about 40 to 100 welding engineers a year. Maybe 40 at Ohio State. There's Ferris State College in Michigan, and LeTourneau College in Texas. Some of these are more like two-year colleges than four-year colleges. The Soviets supposedly produced 5,000 welding engineers a year. Welding engineers are at a premium here. Most of the people in welding are just misplaced metallurgists or physicists or civil engineers, because their boss came to them after a major failure that cost the company tens or hundreds of millions of dollars and said, "We're going to study welding and we're going to fix these problems." It's not a question of not knowing what the problem is — in most cases, we actually know what the problem is. It's just that the people working on it didn't know what the problem was.

§5. The limits of joining: aluminum cars, composite tanks, and the value of a pound [20:23]

§5.p1

So welding is poorly trained for, and applied as an art often before we know the science behind it. Basically, I've made my career by trying to figure out the science behind what people have been applying as an art. When Comfort Adams started the American Welding Society in 1921 after being in charge of building ships in World War I, he came up with the AWS motto: "to foster the art and science of welding." So they admit it's an art.

§5.p2

The last thing I wanted to mention is that our ability to join a material limits the usefulness of the material. [Tom holds up two pieces of aluminum sheet metal.] Here are a couple of pieces of aluminum sheet metal that came out of the automotive research labs — this one at Chrysler, this one at Ford. These people have been trying to build all-aluminum vehicles for 80 years. We built an all-aluminum Duesenberg in the 1930s. And Mellon, of Mellon Bank — I can't remember his first name — was one of the richest men in the United States. He was on the board of Alcoa, and he had this luxury vehicle made out of all aluminum, but only he could afford it.

§5.p3

Twenty years ago I used to hear that because of the increase in the price of gasoline, steel was on its way out, and in a few years we'd all be driving aluminum automobiles. Actually, one of the reasons I wrote that paper on the future of metals was because in the early 90s you'd go to a conference and people would say, "Well, we're not going to be using metals anymore. It's all going to be ceramics." They were trying to make internal combustion engines out of ceramics — they wouldn't have to cool them, they could just take the heat themselves. So I came up with this plot, a fracture mechanics plot of steel versus titanium versus aluminum versus plastics and composites and ceramics. If you study this plot, you want to be way up here, and steel has better properties by an order of magnitude compared to titanium and aluminum. The properties of steel are much better. It's also less expensive.

§5.p4

I also talked about ceramics, because people would say we're going to use these other materials and steel is a dying material. It's not a dying material. I used to say, "In 20 years we'll still be driving steel cars." People said, "What about the all-aluminum Audi?" If you go buy an Audi, it'll be all aluminum — high performance, lightweight. And what will you pay for it? $100,000. If you buy a Ford Taurus, you'll pay $20,000 or $25,000. In the mid-90s I started saying anyone can build a $100,000 vehicle out of aluminum, but building a $20,000 vehicle out of aluminum is a lot more difficult. That's still true today. Twenty-five years ago I predicted we'd still be driving steel cars in 20 years, and here it is 25 years later and we are. All it took was understanding something about joining technology and the cost of materials.

§5.p5

We also couldn't use ceramics because it was hard to join them. We can join them now — if you're willing to pay the price. [Tom holds up a piece of the X-33 space plane hydrogen tank.] Here's a piece of the X-33 space plane. This is all composite — Nomex, which is the same thing as Kevlar but from a different manufacturer than DuPont. You can buy this foam Nomex, which is like Kevlar — fire-resistant. The suits for firemen are made of Nomex; you pay $300 for a jacket rather than $100 because it won't burn very well in a fire. Carbon fiber composites, adhesively bonded. They built this structure on a fast track. It has a foamed adhesive joint through here. They built two of these. That was supposed to be the liquid hydrogen tank for the X-33 space plane. They built them at about $50 million apiece, and they weighed about 4,000 pounds — so it cost about $12,000 a pound to fabricate. What I'm holding is less than an ounce; it's not even $1,000 worth of product.

§5.p6

So most materials can be joined if you're willing to pay the price. But the advantage of steel is it's much cheaper. I handed out last time "Materials for the 21st Century" — that article is my Cliff's Notes version. I was on this committee. They didn't like what I said, so they put all my stuff in the appendix. This is where we talked last time about the relative cost of materials: materials are 10 to 20% of the cost, fabrication — forging, machining, joining — is 20 to 40%.

§5.p7

I also talk about the value of a pound saved over the life of the vehicle. With gasoline at $1 to $2 a gallon — you can see this is a little bit old — you'll save $2 over the 100,000-mile life of a car for every pound you take out. At $4 a gallon, you'd need to go 200,000 miles. The price of the car has gone up since then, too. For an aircraft, they have vice presidents determining how many magazines can be carried, because over the life of the vehicle every pound costs $200. They don't carry very many magazines in first class anymore. American Airlines used to have essentially a clean aluminum skin with no paint, because paint has weight, and at $200 a pound for all those gallons of paint on the fuselage, just to make it look pretty, it adds up.

§5.p8

Over the life of a spacecraft, that piece I just sent around, $20,000 a pound is what it costs to get payload up into space. So you can afford to pay $12,000 a pound for your liquid hydrogen tank — if it works. Except it didn't. But that's another story. Ships and railroads are at about 20 cents a pound as the value of a pound saved. So the ability to join things limits the usefulness of the material, and the cost or value of the material limits the usefulness of what we're using it for.

§6. Show-and-tell: bulletproof glass, gas pipe, laser welds, brazed diamond tips [29:44]

§6.p1

That's the introduction about materials. If we talk about different products — [Tom passes a metal-wood golf club around.] Here's a metal wood.

§6.p2

[Tom passes a piece of bulletproof glass around.] Here's a piece of bulletproof glass. It's not just glass — it has glass in it, three layers, and a layer of polycarbonate, all adhesively bonded. The adhesively bonded joints have to be void-free, because otherwise you're looking at a bubble. The major military vehicles actually have something almost five inches thick, and the presidential limousine also has something about five inches thick, so it can take a shaped-charge weapon, an anti-tank round. It's laminated material — just to make transparent armor.

§6.p3

[Tom holds up a section of plastic gas pipe.] Gas pipe. They used to make gas pipes that run down the street out of steel, but after 30 or 40 years it corrodes, and now you have gas leaking into the soil and you can blow up homes. Now they use plastic — they weld plastic pipe. Very corrosion resistant, but it also fails, and it can fail at the joints. We'll talk about some of that. We talked last time about soldering. I passed around one of the semiconductor chips — an old Pentium chip from the 1995 era. I don't have the newest ones, but the technology of tape-automated bonding is the same, and we'll go through the soldering techniques.

§6.p4

[Tom passes a laser-welded aluminum part around.] This is a laser weld. These are little prototype welds. This one came from a factory in California where they would fill this with explosive — for the canopy of a fighter jet. If you lost electrical power and needed to eject, you don't want to try to eject right through the polycarbonate canopy, because you'll just kill yourself — you won't break the polycarbonate. You also can't rely on having electricity to operate things. So they have a percussive explosive: instead of transferring energy to bolts that hold the canopy on, they have a little aluminum tube filled with explosive, and you can hit the end of it and eject the canopy, then eject yourself. Laser-welded aluminum.

§6.p5

[Tom passes a brazed diamond-tip asphalt tool around.] Here's a brazing example. This is part of a tip for reclaiming asphalt from the street. You may have seen them late at night on the highway — a great big machine with a bunch of these tips going around in circles, beating up the asphalt so they can resurface the road. The tip is usually made out of tungsten carbide, which is one of the hardest materials we know, but you can get a much better life if you use sintered diamond. The black stuff there, about a centimeter across, is sintered diamond. It has to be brazed. So you have to learn how to braze it so it doesn't fail as it beats up the road to reclaim the asphalt.

§6.p6

[Tom holds up a diffusion-bonded titanium part.] We use diffusion bonding. This is a piece of titanium that was part of the development project for the F-21 [F-22] jet fighter. One of the students who was in the class gave this to me — he had recovered it when he was working at Pratt & Whitney research labs, and they were developing the engine and the joining technology of how to put together the jet engine. That's a type of diffusion bonding.

§6.p7

I've got lots of little trinkets up here, and we'll pass them around as we get to these things. So welding is used for all kinds of manufactured products. In a sense, this is a manufacturing course. In another sense, it's a course where I want to prove to you that you already know the answer. You learned in high school chemistry and physics, and someone just has to show you how to think through the problem. Any questions before I start the first subject, which is cold welding?

§7. Why don't two atoms bond when you touch them together? The Lennard-Jones potential [35:19]

§7.p1

So if we go to cold welding — but even more basic: if I take two materials and just touch them together, they don't bond, right? Why don't they bond? There are two fundamental reasons, and throughout the next 11 lectures we're going to keep coming back to these two fundamental reasons why things don't bond when you stick them together.

§7.p2

The first one is: you can think of welding and joining as the opposite of lubrication. In lubrication, you don't want things to bond. What do we do in lubrication to keep things from bonding? We put a film of oil in there, or we put some grease in there. We contaminate the surface with something else that doesn't want to bond. It turns out most materials, if they're clean, want to bond. If I bring two atoms together in an ultra-high vacuum and stick them together, they will bond with considerable force — equivalent strength of 2 million PSI. We don't have anything on Earth, even solid single-crystal diamond, that's that strong. But if I just talked about the bond strength of two atoms, perfectly clean, just brought in contact with each other, they would bond.

§7.p3

Why is that? If you took 3.091 — how many of you took 3.091? One, two, three. Did you learn the Lennard-Jones potential in 5.11? Okay, fine. [Tom puts up an overhead.] Let me show you the Lennard-Jones potential. I'm using some of my old lecture notes. The Lennard-Jones potential is nothing more than the energy potential between two atoms — that's what these little green things are — at some radius. There's some inter-atomic spacing. In a simple cubic system, it's the lattice parameter. In body-centered cubic it's the square root of 3 over 2 times the lattice parameter; in FCC it's the square root of 2 over 2 times the lattice parameter. But in any case, there's some inter-atomic separation, and there's some energy of attraction — as something is far away, you bring it in, you reach a minimum of energy, and then it starts repelling as you get closer.

§7.p4

A student asked me about 15 years ago, "Well, you say it's 2 million PSI — how do you get that?" You go to the Lennard-Jones potential, which you find in any physical chemistry text. The energy is something over r to the n power minus something over r to the m power. One's attractive and one's repulsive. The attractive force is minus a over r to the sixth, and the repulsive force is even greater. Not the energy — the force is the derivative of the energy. The force is zero at the equilibrium spacing; at the equilibrium spacing, it doesn't have anything trying to pull it one way or the other, so the force goes to zero. That's also the minimum of the energy of the Lennard-Jones potential. It's called the Lennard-Jones potential because these quantum mechanics guys in Britain in the 1920s — I don't know if it was one Lennard-Jones with a hyphenated name, or two people. But in any case, there are these potentials for bringing two atoms together.

§7.p5

If you integrate the area under the force curve to pull them apart — F times d, F times dr from zero to infinity — you'll come up with a force to separate those two atoms. I did this for iron, and we'll talk about it later, but you get about 2 million PSI.

§8. Dislocations: why real metals are ten times weaker [41:33]

§8.p1

But in fact, most materials don't have anywhere near that strength. Real iron might have one-tenth that strength. Why is it so much weaker? Student: Defects — dislocations. Right.

§8.p2

You've heard how dislocations were discovered, haven't you? There were two guys. There was Egon Orowan, who was in Hungary at the time as a professor in an institute and later came to MIT as a professor of mechanical engineering. The other was Polanyi — I can't remember his nationality, but I think he was in Britain at the time. People in the 1930s were trying to understand why metals — the physicists had done quantum mechanics, Lennard-Jones had come along in the 1920s, they had done this type of calculation, and they said, "Oh, metals have a strength of 2 million PSI." And people said, "No, they don't."

§8.p3

So in the 1930s they said, "We must have crystal defects that weaken the material." It was Orowan and Polanyi, both independently, who came up with dislocations before we ever saw them. When did we first see dislocations? Not until we got electron microscopes. The first guy to demonstrate them was someone in the 1950s who did very fancy etching techniques on lithium bromide crystals. He could show movement of dislocations — he could etch the dislocations, stress the material, re-etch, and see the movement of the etch pits.

§8.p4

Egon Orowan told the story of how he learned about a dislocation. [Tom tears a sheet from a pad of paper to demonstrate.] He had a very big office with a great big Persian rug. He was working in his office and the cleaning lady came in and noticed that the rug needed to be moved about three or four inches. He said, "I'll help you." She said, "No, I don't need any help." So he watched her. She put a little fold in the rug, like this, and she kicked it across the room, and when she was done the rug had moved a couple of inches. Orowan looked at this, and he thought about it some more.

§8.p5

I used to rip telephone books, but the problem is they're now using plastic-improved paper, so it doesn't rip as easily as the old brittle paper. If you take a telephone book and put a dislocation in it like that, and then you stretch it, you can break it one page at a time. You're just putting a dislocation in and bending it. I put the U in it, I grab it tight, and when I straighten it out, the top page is in tension but all the others are loose. By bending it, I'm ripping one page at a time. That's a dislocation. Analogies are never perfect — I'm not dealing with atoms, I'm dealing with paper. But I used to love the old MIT telephone directories — then they improved the paper, and now we don't even have telephone directories. Science marches on.

§8.p6

So people predict tremendous strengths, and in the 1950s they actually found single crystals of iron. They grew iron whiskers and they had a screw dislocation right up the middle with no edge dislocations — a perfect crystal except for the screw dislocation. If you pull parallel to a screw dislocation, what's the force on the screw to move the dislocation? Zero. If you pulled an edge dislocation in tension, it'd be just like the cleaning lady in Hungary that showed Orowan about dislocations. But a screw dislocation — if you look at the Burgers vector — does anyone study dislocations anymore? I had to take a whole graduate course in dislocations. It was horrible. If you actually study dislocations, you find that a material might lose 90% of its strength because of the movement of dislocations.

§9. Bucky balls, nanotubes, and the trap of forgetting history [46:35]

§9.p1

Today we have great physicists who wanted to win the Nobel Prize for discovering bucky balls — three-dimensional carbon structures. [Tom holds up a diamond-structure model.] This is the structure of diamond. Bucky balls are essentially hollow spheres with sp3 hybrid bonding. They calculated the strength of carbon-carbon bonds and found these should be 3 million PSI, and we're going to be able to make composites out of bucky fibers — nano fibers. That's true — as long as you don't have any defects in those carbon nanotubes. What's the probability of having a defect in a carbon nanotube? Pretty high. If you make them at absolute zero, you can make them without defects, but at any temperature above absolute zero, statistical mechanics will prove to you you'll have some vacancies. And if you have some vacancies, you're going to find they're not as strong as you thought.

§9.p2

So in the last 25 years, the physicists and many materials scientists have sold a billion dollars worth of research on carbon nanotubes, because in theory they're super strong. But who has ever measured the strength of a carbon nanotube? No one. We did measure the strength of asbestos fibers — about 700,000 PSI. Iron whiskers, about 1.2 million PSI. They're not quite as strong as we calculate, but people have been running around selling schlock in materials science because they can't remember history. There was a guy up at Harvard named George Santayana — anybody ever heard of George? He was a philosopher, famous for the quote that those who cannot remember history are condemned to repeat it.

§9.p3

The materials scientists and the physicists — someone won a Nobel Prize for discovering bucky balls, and just a couple years ago someone won a Nobel Prize for forming these flat sheets of bucky films [graphene]. They're all saying, "Oh, this is going to save the world. We will have things that are 10 times as strong." Yes, if they are defect-free. They're not defect-free. So they're actually going to be one-tenth as strong, or one-fifth as strong, when we make them in high quantity, and people are going to be disappointed. So don't invest in carbon nanotubes for structural applications. I'll see you again tomorrow.

Cases referenced

Layer 2 — cleanup edit
p1 00:06

So, in any case, last time I was given the introduction of why I've studied welding and joining over the years, and unfortunately the list has gotten longer and longer. Um, and so I can't even do it in one lecture. But last time we talked about the fact that studying welding and joining is integrative. It uses lots of uh interdisciplinary fields. It's not just a materials field. It's physics, chemistry, structures, civil engineering, mechanical engineering, electrical engineering, chemical engineering. It's a whole bunch of things. Uh welding is about 150 years old in terms of electric uh arc welding and things. It goes back thousands of years to people using uh forges and such things and soldering and things like that.

p2 00:54

Uh it's ubiquitous. Um very few manufactured products that don't contain a joint. In fact, any material that uses two dissimilar materials has to have a joint between the two materials. So, you have to have a monolithic material and if it's a standalone product useful in its own right rather than just a paper weight, it's usually something fairly large. For years, I got pieces like things like needles and things like that. One student came up with a cast iron frying pan. Uh, Professor McClintock came up with an anvil. Has anyone come up with anything any larger? Turns out uh, Professor Pelloux [?] heard this once and he came up with an anvil, but it was the anvil of a forging press and it was about, um, a thousand tons. So, he may win the prize, okay, for the largest uh, standalone object. It was a huge casting.

p3 01:55

Um there are many failures and this is kind of where we stopped the last time. Uh I think I mentioned the when I heard about the space shuttle Challenger what in 1986 or whatever, my students told me about it that morning and I said oh I bet it failed at a weld and I was wrong but it did fail at an O-ring joint. Okay, it was at a joint and we talked about typically things fail at joints because they're the highest stress locations in the structure. It's just sort of natural. Um they also may not be 100% efficient depending on the material.

p4 02:30

Um and we didn't go through all the others, but there's some huge failures that cost a billion dollars or take lots of lives. I don't think I mentioned it. There's an offshore oil platform that I talk about in one of these lectures called the Alexander Kielland about 1980 in the North Sea. This was supposed to be a production platform uh for oil in the North Sea and they changed it to a hotel and a great big storm comes by and these things should have been safe in a storm but the whole thing capsized in the storm and over 200 people died um uh from that accident. And when it was all done, they did the analysis and they found that the French shipyard that had built this offshore oil platform, someone had taken a like a 16-inch diameter piece of steel and welded it to one of these legs. And one of these legs on an offshore oil platform be a big piece of round steel about the diameter of this room. Okay. And they had welded this thing about 16 inches diameter, a little bit bigger, about a basketball size, and they were going to put a sonar uh instrument on there.

p5 03:48

Well, this wasn't, no one thought this was a critical part of the structure. The management of the shipyard uh had one group of people who worried about welding steel that went into the main structure, these great big um circular legs, 24 feet in diameter. And um they let the maintenance people worry about welding the hanger on pieces like this sonar bracket. Well, it turns out they just went to the shop and they got a pipe. It turns out it was a high-carbon steel pipe. And if you weld high-carbon steel, it's very easy to get cracking. They had a little crack about the size of your thumbnail. Uh no one found it because it wasn't a critical part of the structure. After all the inspection was for the critical parts of the structures like the welds in these great big 24 foot diameter legs. No one found it. The waves came along and over time a fatigue crack grew and it grew to where it was 20-some feet long before the storm came by and this 20 foot long crack just snapped it. Um and that's what caused the accident. There's a lot of other things that caused the accident. If you look up the Alexander Kielland was the name of this platform, um you'll find all kinds of stories and a lot of people said the cause of the accident was the fact they didn't have enough lifeboats and things. Well, you didn't need lifeboats if the structure hadn't failed. So, it's question where you start your accounting of the accident here.

p6 05:18

So far as that goes, um, we talked about, um, I think briefly I mentioned I handed out a paper on the future of metals and pointed out that iron and steel constitute 95 pounds out of every 100 pounds of metal made in the world. Aluminum is less than 2%. Iron and steel is about a billion tons a year. And so aluminum at 2% of that's about 20 million tons a year. That's a lot of aluminum, but it's nothing compared to the amount of steel. And so we will talk particularly in fusion welding a lot more about iron and steel because it's the dominant material. And in material selection, you'll hear about why it's the dominant material.

p7 06:08

Um welding is often applied as an art. Um, I often point out that as soon as someone gets a new heat source, they often try to use it to weld. Um, and people discovered over the ages how to do soldering and how to do brazing on art objects and things like that. They even learned to do diffusion bonding. When we get to diffusion bonding, I'll tell you the story about how um the Etruscans used to use tin to bond gold beads to copper objects. They just put them in a furnace and they ended up getting a type of diffusion bond. And I always say the Pratt & Whitney patented this process uh in 1972 only because the Etruscans who used it in 600 BC didn't file an infringement. Okay. Uh against them. Some people think that King Tut's dagger had the same type of beads, gold beads attached to it by this type of diffusion bonding. No one knows cuz no one's willing to cut up the dagger to find out. Okay.

p8 07:14

Um but in any case, welding is often applied as an art. Initially, it was used as an art to make all kinds of vessels and things. Um if you go to Ko— uh Kyoto Japan there Sumitomo I think it is has this museum of Chinese castings. Sumitomo is a metals company in Japan and 5,000 years ago the Chinese were making bronze castings. Well those bronze castings they had to weld on legs and things like that. Well, they did it by pouring molten metal between the leg and the other casting to make a more complex uh product. Um and so they people would use this as initially as an art. Later they used it in the middle ages. A lot of the thing that was driving uh joining technology was um military needs. Um then people started discovering new types of science. Humphry Davy discovered the arc, gave the name to the electric arc in 1805 or 1806 and he tried to weld with it within the next year.

p9 08:30

Um the earliest commercial use of a laser was in the mid mid-50s. The lasers were only invented in the mid-50s, but it's my understanding that General Electric used to make— well, back in the mid-50s, people used vacuum tubes in their electronics. We didn't have silicon yet. Silicon had been invented in 19— as a semiconductor in 1947, but it really hadn't been commercialized. So, most of your power electronics had vacuum tubes. And some of these vacuum tubes would cost a couple hundred or $1,000. And back in 1950, that's a lot of money. And so they might make some of these things and uh seal them in the vacuum and then find out that one of the joints had failed. And suppose General Electric took a research laser and they would— you'd have these two tungsten wires or molybdenum wires inside the vacuum, the clear glass vacuum tube, and supposedly they would first hit it with a soft electron uh laser beam that would just soften the wire so it would make contact with the other wire and then they come in with power and weld it back together to make the electrical connection and repair this thing without having to cut it apart and save the vacuum tube. So, lasers were used early on. Electron beams were used early on within the first uh 5 or 10 years of their having been developed into high power devices.

p10 10:02

In my own experience, um particle beams have been used for welding. Um actually my own experience even before that in the mid-70s, the— they were making high power lasers for military applications but over here in Everett Massachusetts uh it's now Mellon Bank building but they used to have AVCO Everett research laboratories in that building and they had 25 kilowatt lasers that had been developed um for commercial applications under government contracts and they try to laser weld heavy pieces of steel and other materials. Um, the problem with that is I had one of my students went to work for him and he said his main job was making sure the thing worked, the laser worked when one of the customers would come to come in to look at it cuz 90% of the time it didn't even work.

p11 10:57

Um, but they used high power lasers early on. In my experience more directly, in the early 90s, um they had particle beam weapons and the military had spent a quarter billion dollars developing these proton beams that they would supposedly going to— the Navy was going to shoot through the air and shoot down a me— missile coming towards the ship. Um, in the British Falklands war, uh, Falkland Islands war in the 80s, a French Exocet me— missile was fired by the Argentinians on the British carrier Sheffield and it hit the Sheffield cruiser and an aluminum fire started. Debates on whether it was aluminum fire, but it probably was, but it wiped out the entire ship. So, one small missile that you could buy from arms dealers uh anywhere in the world uh could wipe out a capital ship of one of the world's major navies. And so, people were worried about that. So, the US Navy was trying to develop these particle beam weapons from the mid 80s through uh the early 90s and then peace broke out with the former Soviet Union. And so they weren't quite as concerned about it, but they had spent a quarter billion dollars and they wanted to find some application. They had a 3-day workshop, invited me to it, and said, "Can we use these to weld nuclear submarines?" And I went down and said, "Well, maybe you can melt a nuclear submarine, but with 5 megawatts of power, you don't need that to weld. You only need a few tens of kilowatts."

p12 12:31

But anyway, I got a research project in the mid '90s to see if we could use particle beam weapons to do welding and heat treatment and things like that. So as soon as a new technology for heat source comes along, people use it and unfortunately they don't necessarily understand it. So welding is often applied as an art and along with that relatively few people have been trained in welding. It is an interdisciplinary field. If you go back to the top thing there. Um, and so there are people who are materials engineers who like myself, I went to work for a steel company. They said, "You're a welding engineer." I had never taken a welding course in my life, but I was all of a sudden a welding engineer. And I met many physicists who their manager will call them in and say, "You're now a welding engineer." Okay? They they took physics classes. They didn't know anything about welding. And you can kind of see how they kept reinventing the wheel because they took what they knew from physics and would try to apply it to welding. It doesn't always work. Okay, the physics of welding is a little different than what you learn in the classroom.

p13 13:41

So, it turns out there are very few people trained in welding, uh, at least in this country. There's one school that gives a 4-year degree from a regular university. That's Ohio State University for the last 60 years that's had a welding engineering department, but it's actually that department is now folded in with a couple of other departments. Highest paid students in the school of engineering at Ohio State. They take courses in welding and industry wants them. If you go to some place like the former Soviet Union, they had the Paton Institute in Kiev. And for political reasons, which I might explain later, the Paton Institute used to get huge amounts of money from the Soviet government. And so it's an institute of 10,000 people studying welding. Okay? Except they study lots of other things like casting and other things.

p14 14:40

Actually, I'll tell you the story. Uh, Professor Paton, who I think he just passed away a year or two ago, but his father had weld repaired tanks, Soviet tanks during World War II and got them back to the front to fight Hitler. And so he was a hero of the Soviet Union. And after the war, you had the Stalin regime and Paton was a hero of the Soviet Union, and his son took over in the 40s and 50s this uh Paton welding institute named after the father. Now, it's kind of fuzzy if it's named after the father or the son, but anyway, uh, Professor Paton was head of the Ukrainian Academy of Sciences. And in the former Soviet Union, all the research money from the central government came through the Academy of Sciences and was divvied up and there were only seven people on the Soviet Academy of Sciences and Professor Paton was one of those seven. The Ukraine was the largest province, most um financially successful of all the provinces in the uh former Soviet Union. And so they got more research money than any other province because Professor Paton represented Ukraine and when the money came to the Ukraine, he gave most of the money to his institute. Okay, here's corruption at its best.

p15 16:07

And so they had a huge welding institute in the former Soviet Union and they developed technologies like— if you've ever— anybody ever read The Hunt for Red October or seen the movie? In The Hunt for Red October they had titanium submarines. My first research project um in 1977 was from the US Navy to weld titanium for submarines. Here's one of the welds that we made back in 1977 or 78. This probably auto belongs in the Smithsonian. Now, we were welding 1-inch thick titanium for submarines. The United States wanted to build titanium submarines. We never built a titanium submarine other than the deep sea research vessel Alvin that, you know, went down and found the Titanic and things like that. Um, and the Navy built that as part of a prototype program to learn to weld titanium for bigger ships because titanium submarines have the same strength to weight ratio problem that aircraft and all kind of fast-moving vehicles have. In their case, you want high strength to weight so you can dive deeper and hopefully if you lose power, you pop to the surface rather than sink to the bottom because if you sink to the bottom, everything gets crushed, including the people inside.

p16 17:35

So, the Soviets actually built a titanium submarine. And this is a weld made at Oregon Graduate Center by one of the processes that was developed by Dr. Gurevich [?] at the Paton Institute because they spent hundreds of millions of dollars. We couldn't justify building the titanium submarine or spending the money to do the research. But the Soviets were under a different economic system and they were driven by the military needs much more than we are. And so they built a titanium submarine. Turns out it was somewhat of a disaster and within two or three years they all just parked them in the harbor because they were developing leaks and things and I remember the Navy— US Navy asked me, he said how did the Soviets solve the creep fatigue interaction of the titanium? Titanium has this problem that if you put it under compressive stress, a continuous compressive stress, even at room temperature or seawater temperature, it will start to slowly creep. And then if you flex it, there's an interaction. And so the cracks grow ultra fast. And I said in 1980 when we learned about the Soviet Alfa subs, you know, I went to some workshops and um they said, "How'd they solve the problem?" I said, "I don't know." Well, it turns out they didn't. Okay? They built these submarines and they had cracks. Okay? So, they had to park them.

p17 19:08

But anyway, uh the US Navy's never built them uh for various reasons, mostly economic in our case. But the poor training in this country, we produce about 40 to 100 welding engineers a year. Maybe 40 at Ohio State. And there's Ferris State College in Michigan. And then there's LeTourneau College in Texas. Some of these are more like two-year colleges rather than four-year colleges. And they produce welding engineers. The Soviets supposedly produce 5,000 welding engineers a year. Okay. Well, turns out welding engineers are at a premium. But in fact the quality of the training of most of the people in welding, most of the people in welding are just misplaced metallurgists or physicists or civil engineers because their boss came to them. They just had a major failure. Cost the company tens or hundreds of millions of dollars and someone's decided we're going to study welding and we're going to fix these problems. It turns out it's not a question of not knowing what the problem is. In most cases, we actually know what the problem is. It's just the people working on it didn't know what the problem was.

p18 20:23

Anybody have any question? Did you have a question? You're just— okay. Waving your pen. Okay, that's fine. Okay. So, it's poor training. It's applied as an art often before we know the science behind it. And basically, I've made my career by trying to figure out the science behind what people have been applying as an art. When Comfort Adams started the American Welding Society in 1921 after being in charge of building ships in World War I, he basically um came up with the American Welding Society— society is to foster the art and science of welding. Okay. So they admit it's an art.

p19 21:01

The last thing I wanted to mention is our ability to join a material limits the usefulness of the material. Um, here are a couple of pieces of aluminum sheet metal that came out of the automotive research labs. This one at Chrysler, this one at Ford. And the thing is, these people have been trying to build all aluminum vehicles for 80 years. We built an all aluminum Duesenberg in the 1930s. And there's a picture of uh another vehicle with um Mellon of Mellon Bank. Can't remember what his first name is, but he was one of the richest men in the United State in the United States. And he was on the board of Alcoa. He had this luxury vehicle made out of all aluminum, but only he could afford it. Okay.

p20 22:00

And today, I mean, 20 years ago, I used to say, um, people were talking about because of the increase in the price of oil and everything else, gasoline, that we would— steel was on its way out and that in a few years we'd be driving all aluminum automobiles. And actually one of the reasons I wrote that paper on the future of metals where I talked about the future of metals and talked about the importance of steel was because in the early 90s you go to a conference and people would talk about well we're not going to be using metals anymore. It's all going to be ceramics. Okay. Uh they were trying to make internal combustion engines out of ceramics and you wouldn't have to cool them. They could just take the heat themselves. So I came up with this plot which is a fracture mechanics plot of steel versus titanium versus aluminum versus plastics and composites and ceramics. If you study this plot, steel is— you want to be way up here. And steel just has better properties by an order of magnitude compared to titanium and aluminum. And so it turns out the properties of steel are much better. It's also less expensive.

p21 23:20

But I also talked about ceramics in here and that's some of the reasons I wrote this paper because people would talk about we're going to use these other materials and steel is a dying material. Well, it's not a dying material. I used to say in 20 years we'll still be driving steel cars. And people said, "What about the all— at the time Audi was building an all aluminum vehicle?" In fact, if you go buy an Audi, they'll be all aluminum. Okay? High performance, lightweight. And what will you pay for an Audi? $100,000, right? If you go buy a Ford Taurus, you'll pay 20 or $25,000. And I used to— I in the mid '90s I started saying anyone can build a $100,000 vehicle out of aluminum, but building a $20,000 vehicle out of aluminum is a lot more difficult. And in fact, it's true today. And I, you know, 25 years ago I predicted in 20 years we'd still be driving steel cars. And here it is 25 years later and we are still driving steel cars. And it all it took was understanding something about joining technology and the cost of materials.

p22 24:31

Um other things we couldn't use ceramics because it was hard to join them. Um we can join them so far as that goes. Here's a piece of the space shuttle. Uh actually not the space shuttle, the X-33 space plane. This is an all composite material Kevlar. Actually, it's Nomex, which the same thing as Kevlar, but a different manufacturer than DuPont. But you could buy this foam Nomex, which is um like Kevlar. It's a fire-resistant material. They make uh the suits for firemen are made out of Nomex. You know, you pay $300 for a jacket rather than $100 for a jacket made out of Nomex, but it won't burn very well in a fire. Hopefully protect you. It's got carbon fiber composites, adhesive bonded. They made this structure on a fast track. We might talk about it at some point, but um it also has a foamed adhesive joint through here. Um you can look at that. They built two of those. That was supposed to be the liquid hydrogen tank for the X-33 space plane. And it turns out um they built two of them at about $50 million a piece and they weighed about uh 12,000 pounds. No, they weigh about 4,000 pounds anyway. It cost about $12,000 a pound to fabricate that. Okay. So, you're looking at— I mean that's less than an ounce. So, it's not much more than— it's not even $1,000 worth of product right there.

p23 26:09

Um, so you can— I often say most materials can be joined if you're willing to pay the price. Okay? But the advantage of steel is it's much cheaper. And I handed out somewhere last time material— materials for the 21st century. And I think I mentioned that article on materials for the 21st century is kind of my cliff's notes version for material— [Tom searches for the handout.] Um, so materials research for the 21st century defense needs. I was on this committee. They didn't like what I said, so they put all my stuff in appendix. I wrote this um and this is where we talked last time about the relative cost of materials. Materials are 10 to 20% of the cost. Um fabrication, forging, machining, joining is 20 to 40% of the cost. I talk about the cost of different materials.

p24 27:21

But I also talk about in the text of this thing the value of a pound saved over the life of the vehicle. Um with gasoline at $1 to $2 a gallon. You can see this a little bit old. Okay. But nonetheless um uh with gas you'll save $2 over the 100,000 mile life of a car for every pound that you take out of the car. Okay. So, if $4 a gallon, okay, you'll— you need to go two— 200,000 miles, right? Um well, it turns out the price of the car has gone up since then, too. Anyway, um if you talk about an aircraft, you know, they have vice presidents determine how many magazines that can be carried on the aircraft. Actually, they don't carry very many magazines in first class anymore, uh because it's expensive, $200 a pound. So they have people deciding what type of coffee pictures they can carry on the airplane cuz over the life of the vehicle every pound you add is $200. American Airlines used to have essentially a clean aluminum skin with no paint cuz paint weighs— has a weight to it and it's $200 a pound for all those gallons of paint, okay, that you're putting on the aircraft fuselage to make it look pretty.

p25 28:44

Uh over the life of a spacecraft, that piece we just sent around, $20,000 a pound is what it costs to get payload up into space. So, you can afford to pay $12,000 a pound for your liquid hydrogen tank if it works. Except it didn't. Okay, but that's another story. Um, turns out ships and railroads are at about 20 cents a pound as the value of a pound saved in producing that product. So, the ability to join things limits the usefulness of the material. The cost or value of the material limits the usefulness of what we're using it for. So there's sort of— the after an hour and four— one and a half, one and two-thirds classes that's the introduction about materials. Okay. And we can talk about other things but if we talk about different products here's a metal wood.

p26 29:44

So I don't know if you want— sorry. Um I'm going to pass these things around. I need to find a way to hand it to you. [Tom passes samples around the class.] Here's a piece of bulletproof glass. Okay, the bulletproof glass is not just glass. It does have glass in it. Three layers of glass and a layer of um polycarbonate in here. All adhesively bonded. The adhesively bonded joints have to be void free cuz otherwise you're looking at a bubble. Okay, you can't see very well. It turns out the uh the major military vehicles actually have something it's almost five inches thick. And in fact, the presidential limousine also has something about 5 inches thick. So it can take a shape charge weapon, an anti-tank round. Okay? So it has to be that thick and it's laminated material. So just to make transparent— that's called transparent armor.

p27 30:44

Um gas pipe. They used to make gas pipe runs down the street out of metal, out of steel. But after 30, 40 years, it corrodes and now you have gas leaking into the soil and you can blow up homes and things like that. Now they use plastic. Okay, they weld the plastic pipe. Very corrosion resistant, but it also fails and it can fail at the joints. We'll— we can talk about some of that. Um, we talked about soldering. I passed around last time one of the semiconductor chips. This is an old Pentium chip from the 1995 era. I don't have the newest ones, but the technology of tape automated bonding is the same thing. And we'll go through the soldering techniques they use there.

p28 31:28

Um, this is a laser weld. These are little prototype welds. Um, this one came from a factory in California where they would fill this with explosive and then they would— for the canopy of a fighter jet. You did— if you lost your electrical power and you needed to eject, you don't want to try to eject right through that piece of polycarbonate cuz you'll just kill yourself. You won't break the polycarbonate. So, and you also can't rely on having electricity to operate things. So they have a percussive explosive thing that essentially blows the bolts and instead of transferring the energy to send it to the bolts that hold the canopy on, they basically have a little explosive, you know, aluminum filled with explosive and you can hit the end of this thing and you can eject the canopy and then eject yourself. Laser welded aluminum. Okay.

p29 32:29

Uh here's a brazing example. This is part of a tool. Did I bring the rest of the tool? Yeah, I did. If you want to lug this one around. [Tom passes the tool to a student.] This is part of a— u— a tip for reclaiming asphalt from the street. So, I have a great big machine. You may have seen them late at night on the highway. Great big machine. Has a bunch of these things and it's just going around in circles beating up the asphalt and reclaiming it so they can resurface the road. Well, the tip is usually made out of tungsten carbide, which is one of the hardest materials we know, but you can get a much better life if you use a center— essentially sintered diamond. So, this is a sintered diamond tip. The black stuff there, it's about a centimeter across or so is sintered diamond. Has to be brazed. It turns out it has to be brazed. You don't really need to see this. This weighs a couple of pounds. I mean, if you want to see it, you can see it. Um anyway, so you have to learn how to braze that and braze it so it doesn't fail as it just goes and beaten up the road. Okay. To reclaim the asphalt.

p30 33:41

Um we use diffusion bonding. This is a piece of titanium. This was part of the development project for the uh F-21 [F-22] jet fighter. One of the students who was in the class gave this to me. He had recovered it when he was working at Pratt & Whitney in the research labs and they were developing the engine and the joining technology of how to put together the jet engine. But that's a type of diffusion bonding. Anyway, I've got lots of little trinkets up here and we'll go through them and pass them around when we get to these things. Um, these other two are things we're going to talk about later today, maybe if we get there, but probably be tomorrow.

p31 34:23

And so far as that goes, the schedule is tomorrow we'll have class in the other classroom at 11:00 and I'll be there and then Dr. Belmar [?] will be here on Wednesday and Thursday. Friday I'm coming back from Canada on the red eye. So I'll be here as long as my plane's on time and we'll have class at 9:00 a.m. I should be back by about 7:30 that morning. And I'm used to the red eye. Okay, so that's the introduction. Welding really is used for all kinds of manufactured products. In a sense, this is a manufacturing course. In another sense, it's a course where I want to go through things and try to prove to you that you already know the answer. You learned in high school chemistry and physics and someone just has to show you how to think through the problem. And so, let's— any questions before I start actually the first subject, which is cold welding?

p32 35:19

Okay. Um, and so if I do that, if you don't have any questions, now your chance. If you look at Dr. Belmar's uh handout on the first day, he said that I would lecture on 12 lectures or so on cold welding, soldering, brazing, adhesive bonding, flames, thermal cutting, diffusion bonding, and then there's another module some of you might take uh which is 12 lectures on fusion welding processes. Uh and I've given that lectures in the past and you'll be able to review those but right now I want to start about cold welding but even more basic— if I take two materials and just touch them together they don't bond, right? Why don't they bond? There's two fundamental reasons throughout this, you know, in the next 11 lectures we're going to keep coming back to the two fundamental reasons why things don't bond when you stick them together.

p33 36:32

Okay? And the first one is you can think of welding and joining as the opposite of lubrication. In lubrication, you don't want things to bond, right? So, it's the opposite. Well, what do we do in lubrication to keep things from bonding? We put a film of oil in there or we put some grease in there or we do something like that. We contaminate the surface with something else that doesn't want to bond. It turns out most materials if you have them clean want to bond. If I bring two atoms together in an ultra high vacuum and I stick them together, they will bond with considerable force. Like considerable force is an equivalent strength of 2 million PSI. Okay, we don't have anything on the earth even solid single crystal diamond that's that strong. But if I just talked about the bond strength of two atoms and they were perfectly clean, they would— and I just brought them in contact with each other, they would bond to each other.

p34 37:47

And why is that? Well, if you took 3.091, how many of you took 3.091? One, two, three. You didn't think you took 5.11. Did you learn the Lennard-Jones potential in 5.11? Sure, I did. Okay, fine. Um, you probably did. Um, let me show you the Lennard-Jones potential. I'm using some of my old lecture notes here. So, I actually drew these up on— on an overhead. The Lennard-Jones potential is nothing more than the energy potential between two atoms. That's what these little green things are at some radius. And there's some inter-atomic spacing. You can think of that as in a simple cubic system, it's the lattice parameter. In the uh B— body center cubic, it's um square— one let's see square root of 3 over 2 * the lattice parameter. In FCC it's the square root of 2 over 2 * the lattice parameter. But in any case, there's some inter-atomic separation which is a z and there's some energy of attraction— as something is far away you bring it in, reaches a minimum of energy and then it starts repelling as you get closer. Who knows? Maybe I have a— something out of a book that's better.

p35 39:26

Well, this handout should be in your handouts. Um, a student asked me about 15 years ago, well, you say it's 2 million PSI. How do you get that? Well, you go to the Lennard-Jones potential, which you find in any physical chemistry text, okay? And the energy is equal to something over r to the n power plus something— minus something over r to the n power uh plus b / r to the m power or something. In any case, one's attractive and one's repulsive forces and the attractive force is minus a over r 6 and the repulsive force is even greater. Not the energy— the force is the derivative of the energy. And so the force is zero at the equilibrium of spacing, right? The equilibrium spacing, it doesn't have anything trying to pull it one way or the other so the force goes to zero. That's also the minimum of the energy of the Lennard-Jones potential. It's called the Lennard-Jones potential because these quantum mechanics guys in Britain in the 1920s or— I don't know if it was one Lennard-Jones with a hyphenated name or if it was two people. But in any case, there are these potentials for bringing two atoms together.

p36 40:44

And if you actually integrate this area under here to pull them apart, F * D, right? Integral F— FD or you can go through this F * DR 0 to infinity and you'll come up with a force to separate those two atoms. I think I did this for iron and we'll talk about it later. But you get about 2 million PSI. Okay. But in fact, most materials don't have anywhere near that strength. What about real iron which might have one-tenth that strength? Why is it so much weaker? Pardon me. There's defects, dislocations specifically, right?

p37 41:33

And you've heard how dislocations were discovered, haven't you? There were two guys. There was Egon Orowan who— end up he was in Hungary at the time as a professor in an institute and he later came and became a professor of mechanical engineering here at MIT. The other one was Polanyi and Polanyi was— can't remember— I think he was— I can't remember his nationality but I think he was in Britain at the time. But people in the 1930s were trying to understand why metals— people had done quantum mechanics. Lennard-Jones came along in the 1920s and they did this type of calculation and they said, "Oh, metals have a strength of 2 million PSI" and they were the physicists who had done this and people said no they don't.

p38 42:17

And then people started postulating why. So the 1930s they said we must have things that are crystal defects just like you said— defects in the crystals that weaken the material. And it was this guy Orowan and Polanyi who both independently came up with dislocations before we ever saw them. When did we first see dislocations? Not until we got electron microscopes. But the first guy was a guy in the 1950s who did some very fancy etching techniques on lithium bromide crystals and he could show movement of dislocations. He could get etching of the dislocations and he could then stress the material and re-etch it and he could see the movement of these etch pits, these defects in the crystals.

p39 43:08

Well, it turns out Egon Orowan told the story of how he learned about a dislocation and I forgot to bring the sample with me. I guess I could rip a piece of a pad of paper instead. I guess I could sacrifice a pad of paper. He was— he had a very big office with a great big rug, you know, Persian rug in the office. And he was working in his office and the cleaning lady came in and she noticed that the rug needed to be moved about 3 or 4 inches. And she mentioned that the rug needed to be moved. He says, "I'll help you." She says, "No, I don't need any help." And so he watched her. She put a little fold in the rug like this. [Tom demonstrates with a pad of paper.] And she just put it like that and she kicked it across the room and when she was done the rug had moved a couple of inches. Okay. And— and so Orowan looked at this and he thought that's interesting and he thought about it some more.

p40 44:08

I used to rip telephone books but I don't— the problem is the telephone books are now using plastic improved paper so it doesn't rip as easy as the old brittle paper. But if you take a telephone book and you put a dislocation in it like that and then you stretch it, you can break it one page at a time and start the defect. And you're just putting a dislocation and you actually bend it. I, you know, I put the U in it and I grabbed it tight. And when I straighten it out, the top one's in tension, but all the others are loose. And so I basically by bending it, I'm ripping one page at a time. So that's a dislocation— shows— I've had— other factor— that's not the proper analogy. It is the proper analogy. I'm sorry. Okay. Analogies are never perfect. Okay. It's not— I'm not dealing with atoms here. I'm dealing with paper. But if you want— if I can find an old— I used to love the old MIT telephone directories, but then they improved the paper and now we don't even have telephone directories. So what am I going to do? Science marches on. Okay.

p41 45:18

Um, so anyway, people predict tremendous strengths and you know what people in the 1950s actually found single crystals of iron. They call it— they grew iron whiskers and they had a screw dislocation right up the middle with no edge dislocations. A perfect crystal except for the screw dislocation. And if you pull a screw dislocation, if the screw dislocation is this way, you pull parallel to a screw dislocation, what's the force on the screw to move the screw dislocation? It's zero. Okay, edge dislocations. Uh, if you pulled an edge dislocation in tension, it'd be just like the cleaning lady in Hungary that showed Orowan about dislocations. Um, but a screw dislocation, if you look at the Burgers vector and you study— anyone study dislocations anymore? I had to take a whole graduate course in dislocations. It was horrible. But anyway, um, if you actually study dislocations, you find that the material might lose 90% of its strength because the movement of dislocations.

p42 46:35

Today we have great physicists who wanted to win the Nobel Prize for discovering bucky balls, right? And bucky balls are these three-dimensional carbon structures. This is the structure of diamond. But bucky balls are essentially hollow spheres with sp3 hybrid bonding. And they calculated the strength of carbon-carbon bonds and they found these should be 3 million PSI and we're going to be able to make composites out of um bucky fibers, you know, nano fibers. Well, you know what? That's true. As long as you don't have any defects in those carbon nano tubes. What are the prob— what's the probability of having a defect in a carbon nano tube? It's pretty high. If you make them at absolute zero, you can make them without defects. But any temperature above absolute zero, statistical mechanics will prove to you— will have some vacancies. And if you have some vacancies, you're going to find that they're not as strong as you thought.

p43 47:45

So in the last 25 years, the physicists and many material scientists have sold billion— a billion dollars worth of research on carbon nano tubes because in theory they're super strong. But who has ever measured the strength of a carbon nano tube? No one. But we did measure the strength of asbestos fibers which about 700,000 PSI. Iron whiskers about 1.2 million PSI. They're not quite as strong as we calculate, but people have been running around selling schlock, okay, in material science because they can't remember history. And there was a guy up at Harvard named George Santayana. Anybody ever heard of George? He was a philosopher. And he's famous for a quote that those who cannot remember history are condemned to repeat it.

p44 48:43

Okay. And so the material scientist and the physicist and someone won a Nobel Prize for discovering um bucky balls. And just a couple years ago, someone won a Nobel Prize for forming these flat sheets of bucky films [graphene]. Okay. And they're all saying, "Oh, this is going to save the world. We will have things that are 10 times as strong." Yes, if they are defect free, but in fact, they're not defect free. And so, they're actually going to be one-tenth as strong or 1/5th as strong when we actually make them in high quantity and people are going to be disappointed. So, don't invest in carbon nano tubes for structural applications. And I'll see you again tomorrow.