DP_S2012_04

Deformation Processing Spring 2012 Session · 9 sections 13 cases · Watch on YouTube ↗ all files
Layer 3 — readable edition

§1. Schedule note and the Blackhawk washer follow-up [00:04]

§1.p1

Next Tuesday is actually Monday at MIT — they do this once every spring term so the schedule gets the right number of Monday-Wednesday-Friday and Tuesday-Thursday classes, and the way they do it in the spring, they always have to turn a Tuesday into a Monday. So next week I'll be lecturing Tuesday and Wednesday in this room at 9 o'clock. If you go to 26-100 at 11:00, have fun. The videos are going up within a day or two now; we had some problems earlier this week but I think it's all resolved. Simone will be doing both Thursday and Friday of next week.

§1.p2

We talked about the Blackhawk washer two days ago, and I brought a couple of my little pieces left over from fifteen years ago. [Tom produces the washers.] This is the washer, and fifteen years ago it cost $350. This one's painted gray — that means it's a Seahawk. This one's green, it's an army part. This one's steel, this one's aluminum, don't ask me why. It's a very clever design. In order to keep it tight, there's a different number of holes in this than in here, and so no matter how you turn it, within about two or three degrees you always get one hole to line up, and they put a screw in there to keep it from loosening. They don't use lock wire or friction; they have a positive thing, because if you lose your tail rotor you just spin to the ground, which is exactly what happened.

§1.p3

But the reason they lost their tail rotor is this washer. In the incident, one developed a stress corrosion crack. We took this one which had never been used — the reason there's a saw cut there, we measured the distance very precisely, within a fraction of a thousandth of an inch. There are flats here that keep it from rotating. Then we made the saw cut and measured the distance again, and depending on whether it shrinks or opens you can calculate — it's basically just a simple circular beam — how much stress it took to open it or close it. We measured 8 ksi residual stresses in this part. With the heat treatment for the alloy it's made out of, 5 ksi would cause stress corrosion cracking. The solution was to go to an overaged T73 heat treatment, which has a stress corrosion cracking minimum of 25 ksi. So they had been making it out of something that was only good for 5 ksi resistance; they switched to 25 ksi material, which is just a heat treatment change, not a compositional change. The residual stresses were 8 ksi, so everything fit together.

§2. Necking, voids, and inclusion control [03:38]

§2.p1

Now, a question — I wish I had brought Backofen with me, but fortunately they didn't erase my wonderful drawing over here. We were talking about necking and void formation in a tensile test, and these are graphs out of Backofen. You're doing a simple uniaxial tensile pull; here's the fractured specimen, here's necking. If you cross-section a piece of copper and do metallography, you find a bunch of voids forming in the neck. The neck goes into a state of triaxial stress — we'll talk about stress states later, but it's basically hydrostatic tension, and that's what helps the voids open up. The whole thing's being pulled in all three directions. At higher magnification you see these elongated voids, and you can see copper oxide particles — these little black spots are inclusions — and in the holes they're acting to nucleate something.

§2.p2

This, I think, is out of Hosford. It may be in your book. Hosford has some pictures and you can see the fracture in the neck, what we call ductile dimple rupture. This is a cross-section, and you can see the cross-section of the dimples and how the voids are forming, pulling apart. Classically, this is looking down on the fracture in the scanning electron microscope, and you see the ductile dimples like taffy pull at 3,000x. Inside many of these you'll see the oxide inclusions that are nucleating each dimple. That's classic ductile rupture. I've now preempted Dr. Belmar on ductile fracture.

§2.p3

Backofen has this drawing: if I had something with no inclusions, very clean material, and I pulled on it, it might neck down like this — I get tremendous elongation. As a thought experiment, the inclusions basically break the material up into a bunch of fibers, smaller tensile specimens, and when they neck down it's like necking down a bunch of fibers. The total elongation with inclusions is a lot less than the elongation if the material was very pure. We know that's true. Back in the '60s and '70s, we spent billions of dollars coming up with vacuum arc melting and all these fancy things to get rid of inclusions in metals, because they are crack starters.

§2.p4

All the crankshafts and piston engines and aircraft have to be triple vacuum arc melted now, because vacuum arc melting burns away the inclusions formed from the regular steelmaking process. You make the steel, cast it into an ingot, and then you take that great big ingot and arc it into another mold. You've got a round ingot full of dirt and inclusions, and you arc it into a copper mold, withdrawing as you go — you just remelt it, but in a vacuum. Now in the heat of those little spatters of metal going across, they're being melted in a vacuum, and it sucks out the oxygen and nitrogen, and you end up with a very clean steel. They will triple vacuum arc remelt aircraft landing gear, transmission shafts, and the shafts for turbine engines. They're using steel for these things and triple-melting them — once, twice, and three times. You end up with things so clean you look at them at 500x and have a hard time finding an inclusion. There are standards for all these inclusion counts.

§3. Orange peel and redundant deformation [08:24]

§3.p1

One of you asked me about orange peel. Here's a picture of orange peel — this is from Hosford's book too, probably chapter 16. I don't know what it is — looks like it might have been the bottom of a gas tank in the automotive industry — but it's a drawing from a stamping from sheet metal, and the surface looks like an orange. It's caused by large grain size. Those little pebble surfaces, each one is about the size of the grain in the material. If you want to avoid this — I'm not going to call it a defect, because it doesn't weaken the material, but if you wanted a nice fender on a car, the paint wouldn't cover it up. So it's not generally desirable. You have to control the grain size, and we'll talk about that later.

§3.p2

Going back several days, I was talking about redundant deformation and how you look at the deformation zone geometry. At a delta of one — sheet rolling, straight-line deformation — you have x's in the slip-line field. But at a delta of four or ten, the slip lines all have this curvature. When the slip lines are straight, you have uniform, homogeneous deformation. When they curve at higher delta, you have non-uniform, inhomogeneous straining — redundant deformation. The redundant deformation comes from the fact that you have to bend it one way, then another, then another. I could tell some of the eyes were glazing over at that point.

§3.p3

So here's my example. [Tom produces two decks of cards held together with rubber bands.] If I deform it, I shear. Remember, plastic deformation only occurs in shear. Hydrostatic compression or hydrostatic tension has no effect on deforming the metal. It might allow it to go to higher elongation, but it doesn't cause the shape change. The shape change is due to shear. So if I do a shear on this, that's a delta-equals-one type of shear. At delta equals five, you shear it that way, you shear it back the other way, and then you shear it that way to get the same shape change. You did three times the work to get to the same thermodynamic state. In thermodynamics, the end states are state properties — they tell you the energy or the shape, but they don't tell you the path. Work is not path-independent; work is not conserved. The shear work to go this way, back that way, and then this way again — I get one shape change for three, but I pay the price three times in energy. That's redundant deformation. And a lot of that inhomogeneous flow comes from friction.

§3.p4

This is out of Backofen, and it shows the delta dependence of the inhomogeneity factor for copper strip with different lubrication. Here's delta. At delta equals one, the height and width of the deformation zone are equal — you're really in a rolling situation. Over here you're getting toward drawing or extrusion. You can change the die angle of the draw. Unlubricated, the inhomogeneity factor increases as you get to higher and higher delta. We saw that in the handout I just gave you — the inhomogeneity factor increases when you have less die angle. Then if you've got paraffin oil or soap — and remember, soaps are stearates, and later we'll talk about why stearates are such good lubricants.

§3.p5

We can also talk about why, if you live in an area with hard water and you take a shower, you still feel soapy after you've rinsed off. Anybody live in an area of hard water? You lived where? New Jersey. If you have a lot of calcium in your water, that's called hard water — the amount of calcium in the water is called the hardness. New England has nice soft water; take a shower, rinse off, you feel nice. But in San Antonio or certain parts of New Jersey they're probably using well water, and it gets saturated with limestone and a lot of calcium. The soap is a calcium stearate, and if your water is already saturated with calcium, you can't dissolve off the soap. A monolayer of stearate molecules stays on your skin, and you can rinse till the cows come home and you're still going to feel slimy. I travel around the country, go to a hotel, take my shower, and I can tell you whether it's hard or soft water.

§4. Upset forging and friction at the die [14:57]

§4.p1

Any questions? Now we want to talk about forging-type deformations. This is almost a delta of one, not exactly one but close. Not everybody uses delta — Backofen liked to use it, and his students Hosford and others like to use it, but before the 1960s most people don't talk about delta operations in terms of deformation. This is showing two different friction levels in metal flow. You start with something like this, reduce it 8%, 22%, 33%, 44%, and 60%, and you can see the inhomogeneous deformation. The squares in this rectangle turn into — in the center maybe they're still squares, but at the edges they have funny shapes. As you go further, you get worse and worse uniformity.

§4.p2

This shape change would be a frictionless type of deformation, but you typically have something that causes this barrel shape. If you want to see the barrel shape in the real world — this is Japan Steel Works, doing upset forging of some big heavy piece. Here's upset forging of a big hot piece of steel and you can see it's starting to barrel.

§4.p3

This thing's pretty big — it's a 600-ton forging. The largest forgings we do, or the largest pieces of steel we do, are about 750 tons, so they don't get much bigger than this. Anybody have an idea why it looks kind of whitish right underneath the clamp? Because we broke off the oxide. In order to heat this all the way through, you had to leave it in the furnace for a week — an air furnace at about 2200°F — and the iron oxidizes in the furnace. The oxide's about an inch or two thick after a week at 2200°F. Now you grab it with these big tweezers — they're big tweezers to pick up a 600-ton piece — and the oxide breaks off. The oxide has a different emissivity. When you actually forge this, you'll have this hot slag of oxide and it'll all break off.

§4.p4

I remember the first time I worked for Bethlehem Steel during the summer, they had a program to introduce all the 500 new engineers that year to steelmaking. In the morning we would listen to vice presidents give talks. This lasted for a week, which tells you how many vice presidents they had — you could spend five mornings listening to them. They weren't long talks, half an hour each. In the afternoon we'd go down to the Bethlehem plant. I remember going to the forging plant — this was summer of 1975 — and they had a big forging hammer slamming down on these things. When the great big crane moved the steel back and they were done, two bare-shirted steelworkers went out with their shovels scooping up all the slag, the oxide that had come off. It was about six inches deep on the forging bed, and you had to scoop it off, because if you brought another one in, all you'd do is forge that stuff into the surface of the next one.

§4.p5

It was all done manually, and it was amazing to me. I sat there kind of bug-eyed. They had a dumpster brought up, and one guy would scoop down, come up, and throw it over his shoulder into the dumpster — hot slag at about 1,000°F. The other guy would go down, and they were like pistons going back and forth. I said to a guy, what if one of them got out of sync and threw hot slag in the other guy's face? And the guy says, well, they've been doing it for thirty years. The guys who do throw it in the other guy's face, they probably don't work there anymore, because they may be dead.

§4.p6

The die starts out cold, and by the time you end up forging, the anvil — which may only be four feet thick — and the hammer above, which may be two or three feet thick, you don't want to touch it. It's probably pretty warm; it might get up to 1,000°. You're forging something at 2200, and you're hammering it. Go watch the blacksmith here in the basement. He starts with a cold hammer, hits something hard, and when he's done, that hammer gets warm. But it only gets to about half the temperature of the thing you're forging. If you keep hitting with that same hammer and don't let it cool off, you'll have a problem, because it heats up, and now you're taking one material that's softened by heat and another that's strong by low temperature, and you're using the hard cold material to form the hot material.

§5. Three forming regimes and isothermal forging [21:16]

§5.p1

That's something I was going to talk about next week. There are three ways we can form things. We either start with something that's really hard and form something really soft — remember those little machine screws, that's cold heading. That's all at room temperature, no temperature effect to give me a strength difference. What do I do there? I heat-treat the steel to 200 ksi strength, and the workpiece is going to be 30 ksi annealed steel, soft as I can get it. As I'm working, it gets up, and that final part is probably 100 ksi, but the tool is still 200 ksi. I've got to have good lubrication. So that's a case of same temperature but big strength differences.

§5.p2

Then I can use temperature as the advantage, but now the process isn't isothermal. I have to have a cold tool and a hot workpiece, and I have to have a little time in between for the tool to cool off. That's what you were asking — it gets hot.

§5.p3

The third one is called isothermal forging, and it was developed because of Backofen and superplasticity in 1965, when he rediscovered it from Germany. That's Tuesday's lecture; I don't think we'll get to that today. Isothermal forging is how we make a lot of the turbine discs for airplanes, jet engines and so on. That sample should be in the Smithsonian. I recovered it from a graduate student's desk — they were using it as an ashtray.

§5.p4

Student: Will they just let the forming tool — or do they try to cool it?

§5.p5

No, actually, in superplastic forming you get material that, instead of taking a 30% stretch, will take a 400% stretch. Sometimes you can use graphite dies, which aren't particularly strong, but you get the material up to where it's like clay. You take the nickel-base superalloy up to 2200°F and it will deform like clay. You have to have something that's a little stronger, but it can be something relatively weak, like graphite dies. You can use molybdenum dies, or other superalloys that have a little more temperature capability. You're limited in your die materials, but everything is hot — it's isothermal. The dies are just as hot as the workpiece, and you're using a material that's superplastic.

§5.p6

We'll talk about isothermal forging next time — I have to explain how you get superplasticity first. We could not build the jet engines you fly on today without it. When you fly on United or Delta or American, you're flying in a whole different technology than in 1960 when I flew up here to come to school as a freshman. They may have been jet engines, but they're a lot different.

§6. Nasmyth's steam hammer and stories about Backofen [24:44]

§6.p1

I want to show you one other thing. This is James Nasmyth's painting of his patented steam hammer forging the propeller shafts. This is a 30-inch diameter shaft for Brunel's SS Great Britain — it was going to be one of the largest ships. These were the largest wrought-iron forgings of their day. It was just a steam hammer, big steam cylinder up here, and they're going to take an ingot of wrought iron. This isn't even steel technology, this is wrought iron. Look at the manipulator they have back here — count them, there are actual men moving this thing. You've got an anvil right here. Notice the shape of that anvil — it's V-shaped. Remember, I showed you the picture of how you don't want to do deformation at delta of 5 with just two platens coming together, because you'll crack the inside — it goes into tension. But if you do it from three sides with a V-shaped anvil, you actually get compression in the center, and you don't cause splits in the center. 1839 — they had studied Backofen, they knew all about delta, and that's why they were using their V-shaped anvils.

§6.p2

Someday I have to tell you some stories on Al Backofen. He was an interesting guy. I'll tell you a couple of them right now. When I came back as a sophomore, I had worked 80-hour weeks that summer between freshman and sophomore year. It was during the Vietnam War, and I was lucky enough — I took the civil service test in Virginia Beach, where I grew up, to get a summer job. You had to be able to add two and three rather than just two and two — really hard questions — and I got above a 95, maybe a 98 or 99, which was high enough that I got hired as a postman.

§6.p3

The job I'd had the summer before paid me a dollar an hour as a clerk in a drugstore at Virginia Beach. The post office paid me $3.35 an hour, which was the standard rate. I was replacing postmen going on vacation for two weeks during the summer. My favorite part — later in the summer they had me delivering special delivery letters, like express mail today. This was before FedEx; for 35 cents you could get a letter delivered special delivery. Typically I'd show up at 9:00 in the morning, they'd give me ten or twelve special delivery letters that had to be delivered immediately in Virginia Beach. I'd get in the station wagon and drive for the next eight hours, because Virginia Beach at the time was the fifth-largest city in the United States by area. Chesapeake, Virginia, was the third-largest. They had incorporated whole counties under Virginia law into cities so that Norfolk and Portsmouth couldn't annex them. So they were paying me a little over $24 to deliver $3 worth of mail. And we wonder why the post office is going broke.

§6.p4

The next summer I needed to make my three bucks an hour to pay MIT tuition, so I did the civil service thing again. They hired me at the Naval Air Rework Facility, where they rebuilt jet engines — we had all these crashes coming back from Vietnam and had to rebuild the engines. I was just an engineering trainee, but that was only two bucks an hour, so I took my old clerk job back at a buck an hour, and I worked 80 hours a week at two jobs 30 miles apart. It was not a great summer.

§6.p5

So I came back here and decided I would work in the lab. I'd taken my mechanics of materials class — my first materials course other than 3.091 — Al Backofen was the professor. I went up to him at the end of class and said, Professor, would you have any jobs in your lab? He said, come back to me next week. Well, he came to me at the next class and said, I found a job for you, go see Tony Thompson. So I started working for Backofen. He was a very kind man as long as you weren't his doctoral student. If you were a bachelor's or master's student, he was a gracious gentleman — white hair, always wore a bow tie, kind of bow-tie academic, tweed sport coat. When I started, they put me in that little short door, 8-137 — that was Backofen's graduate students' office.

§6.p6

Backofen was leaving the week that I came. He had retired in his mid-fifties. He couldn't get along with anybody, decided to heck with it, and was leaving MIT just as I was starting. But he had liked me — I'd been one of his undergraduates — and he came to me and gave me a piece of advice: the only way to keep your sanity around here is with a pocket full of Valium. I've always remembered that.

§6.p7

He had a home up in Marblehead. This was 1976, and he and his wife decided they would put it on the market for an outrageous price: $90,000. If anyone offered it to them, they would just move to their farm in New Hampshire. Well, the first person who came by offered him $90,000. He obviously didn't have a clue what the place was worth, and he sold it and moved to New Hampshire. About twice a year he would come back when I was an assistant professor, and he'd always stop by to see me, ask how I was doing. In his later years — he only passed away about two years ago in his eighties — he had started a Christmas tree farm in New Hampshire. This was before you could buy nicely pruned Christmas trees. He'd go out in the spring and spend his time pruning the trees, and he'd sell them for $3 a foot — a 7-foot tree was $21. Ordinarily you'd pay $3 for a scrawny Christmas tree. He was leading the market. He was selling 10,000 trees a year and making about $50,000 or $60,000. My salary was $15,000 as an assistant professor.

§6.p8

The other thing he'd do up in New Hampshire and Vermont and Maine — he'd go to the yard sales and buy junk, then take it to New York City and sell it as antiques. One man's junk is another man's treasure. He told me he was making more money than he had ever made as a consultant or a professor. Backofen was a character. Maybe someone will tell a story about me being a character someday.

§7. Inhomogeneous flow in forging and extrusion [33:06]

§7.p1

I want to start showing you some types of flow you get from inhomogeneous deformation. Here's hot upsetting of steel with sticking friction. Sticking friction means the stuff under the tool doesn't move at all. The material is stuck to the workpiece — all you have to do is not put on the glass lubricant. For steel forging, like I showed you, you don't use any lubricant; you just let the oxide scale fall off. But for a nickel-based superalloy, you encase the whole thing in a glass frit, and when you get it hot, you have this syrupy layer of glass — the glass melts and gets thick, and if you pick the right glass for the forging temperature, it'll be a good lubricant.

§7.p2

This one was done without lubricant, and you can see the material flow lines. Initially, this material right underneath the tool didn't deform at all — it might as well have been part of the tool. You can think of the flow lines as grains of wood in the original billet of steel. It bowed out, and notice how it's curling around. You're going to form a defect — if you kept this going, you'd get a little lap. That's the effect of friction, and you can see the inhomogeneous deformation. This material didn't get worked at all; this material got worked in this direction, that direction, a number of times.

§7.p3

Let me give you another example. This probably comes out of Metal Forming by Altan. This is a titanium blank, which has an alpha-and-beta microstructure initially. It's been squeezed down, and from the etched microstructure afterwards, you can see it looks fairly uniform — little barreling at the ends, but it flowed fairly uniformly. This is an all-beta microstructure. Titanium comes in alpha form and beta form — alpha is hexagonal close-packed, beta is body-centered cubic. If you forge something in the alpha-beta range, good deal, nice uniform product. Try to form it in the all-beta — look what happens. You get shear bands, localized shearing. You've got the big coarse microstructure, and then these bands in between. You see the X from the delta-equals-one type of deformation. The material tried to shear on these simple little X-planes; the X got distorted, but you can see the X. Those are the shear bands.

§7.p4

This comes out of Hosford. One of the things people do is take modeling clay. I'm not kidding. Now they do a finite element analysis in the computer, but in the old days they would take modeling clay, put two pieces together with nice flat surfaces, scribe grids on them, and then extrude the two pieces through the same die. They'd pull it apart, and you could see the flow lines. Here we have different die angles: 40, 45, 60, another angle. This is actually Don Blickwede again, my old boss when he was vice president of Beth Steel. Those may actually be steel billets rather than clay — cold-extruded billets.

§7.p5

If you look at the hardness number — they're looking at hardness at different amounts of deformation, distance from the center. With zero deformation, everything's nice little squares and you have low hardness — if it's steel, let's say Rockwell B 50, very annealed steel. As you go up in deformation from 4 to 6 to 13 to 26, you'll see that initially you get very inhomogeneous deformation across there. Then you get a lot of deformation, and everything becomes homogeneous again because it's all fully kneaded. You've really beaten down that pizza dough. If you're going to make a pizza, it's going to have a uniform crust. These are the practical things in this course. You've got to knead it a reasonable amount. You can't do something in between. If you do nothing, you don't have much. The first stuff introduces a lot of inhomogeneity, and you really have to get to 40% deformation before things start to get homogeneous again.

§7.p6

I used to think, when I was a bachelor's student here doing wire drawing for my thesis to make superconducting wires, that I would do better with small reductions. I had a great big set of wire dies — you could buy diamond dies for 20 bucks apiece back then. I had a government research contract, so I went out and bought $1,000 worth of dies in 5% increments. That was the wrong way to go. You should be doing 30 or 40 or 50% draws, not 5 or 10% draws, because with 5 or 10% draws you get lousy deltas. High-delta operations let you crack the center, and you also get very inhomogeneous deformation. This is the highest delta operation among these four.

§8. The Acela trolley wire and the Phelps Dodge story [39:28]

§8.p1

If you're going to work it, you've got to work it a lot. I guess I do have another story on that. Here's the trolley wire again. [Tom holds up the trolley wire sample.] This trolley wire has got an equivalent delta of about 30. Super-fine grain — it's actually starting to get into the superplastic region, I believe. Made by Phelps Dodge.

§8.p2

The company that originally bid on this — this was for the Northeast extension of Amtrak, the Acela line from New Haven to Boston. There was a $330 million federal contract to build the line, and that was the product they wanted. They had to purchase somewhere between $4 million and $7 million worth of copper to mount it. I got a call about December 20th or 21st saying, Tom, can you go to Rome, New York? There's a little company making our trolley wire. This is from the Amtrak engineer. We drove out there on the 22nd, and they said, oh by the way, we need an answer before Christmas. That's not very far away from December 22nd.

§8.p3

This company had been making copper wire for years, but the largest diameter they had ever made was 5/16 of an inch. They had never made anything much above a quarter of an inch in diameter. The largest mold they had on their continuous caster was about an inch and three-eighths, and you can see the grains — there's a longitudinal cut and another cut. Huge grains. Remember I showed you the orange peel. If you have large grains and you deform something — Amtrak's question was, are we going to have problems with this large grain size? The company said, well, we're meeting your spec, except we don't have small grains, is that okay? I had to give the answer before Christmas.

§8.p4

On the 23rd I told them to reject the product — $4.5 million worth of product. It turns out it was a fixed-price contract with the US government, and the company had certified to the US government that this company in Rome, New York, that had never made wire bigger than 5/16 of an inch, was the only company in the entire world that could make this trolley wire — because Amtrak had some very tight specs. This is a copper-silver alloy that had to have certain mechanical properties, a certain amount of elongation. I didn't realize all this stuff, but I had rejected it, and Amtrak sent a letter saying we reject it, you can't put this up, you have to find other material. But they had already certified there was no one in the world that could make it to the Amtrak specs.

§8.p5

It so happens that Phelps Dodge, the second-largest copper company in the world, had been begging this company for two years to make a bid on this. The problem was, Phelps Dodge's alloy was so good and had so much redundant deformation and super-fine grain size that — Amtrak for some reason had a spec of between 8 and 14% elongation, and this stuff had 18% elongation. It had too much elongation. It was too ductile. It was too good. Ordinarily you have to meet a minimum, but they had given an upper limit. Why someone said the elongation should be between 8 and 14, I don't know. So this company hadn't allowed Phelps Dodge to bid because they exceeded the maximum, when there should have been no maximum. That's how they had written the spec, and technically they wouldn't let them bid, even though it was going to be a much better product. You've seen the tensile bars — I sent them around — they neck down, big stretch.

§8.p6

Phelps Dodge's price was going to be $6.5 million or $7 million, and this company in Rome was going to be $4.5 million. So the money in the pocket of this British company was going to be an extra $2.5 million of profit if they could convince the government to buy their junk. I'd rejected it, so it goes to a week-long arbitration in December at an ocean resort in Old Saybrook, Connecticut.

§8.p7

This thing goes on forever, but the bottom line was, when they gave the briefings, the attorneys for the British company argued that Tom Eagar was an absolutely insane and incompetent metallurgist to have rejected this material — he had no basis to do it, and it cost us $2.5 million and the government owes us $25 million extra because they forced us to go out and buy the Phelps Dodge material. The briefing from the government was: you committed fraud on the federal government. You told us there was no one else willing to bid on this in the entire world, and we found out that Phelps Dodge has been trying to bid on this. The attorneys from the British company realized they could be sued criminally. And in fact, that's exactly what happened a week after the arbitration. The FBI raided the offices of the British company, took the passports of the senior managers, took their computers. At that point I was out of it.

§8.p8

Don't defraud the federal government. Amtrak has the legal authority to put you in jail if you tell them a lie. Other companies tell lies to each other all the time, but it's not good to do it to the federal government — they can do things. The other part of that story is how we actually won the arbitration. There really was nothing in the literature that said you couldn't do this, that the grain size should be a big problem. But it turned out it was essentially an orange peel effect, a large grain size effect.

§8.p9

Even though Amtrak had told this company, don't you dare install any of that wire, they took about a 10-mile stretch down here in Providence and installed the stuff from Rome, New York. They ran the train along that 10 miles and videotaped it. The pantograph, which is the carbon brushes running along the wire — it turns out there was a rough surface on the wire, and as the thing's going along at 60 mph, it looked like the 4th of July. It was sparking all over everywhere. If they had put that up for a couple hundred miles, they would have had to take it down two weeks later, because it would have eaten itself to pieces from all the electric sparks. And the idiots were smart enough to videotape it for us. I didn't know at the time that was the reason to reject it. I did look at some data — Tony Thompson, who I first worked with under Backofen, had done his doctoral thesis on grain size effects of fatigue in copper, and I went back to some of Tony's papers. So that's another little story of how I got myself in trouble.

§8.p10

Sometimes you just have to make a decision. I wasn't sued directly, but Amtrak was sued for $25 million because of my decision, and we ended up proving ourselves right because they provided the evidence for us. I don't know what happened to the criminal proceeding.

§9. Extrusion dead zones and the Stamixco mixer puzzle [48:19]

§9.p1

This is extrusion. If you go with straight-edged extrusion dies, you can have different types of things going on, but in fact you end up with dead zones. This is what they call backward extrusion — you push a tube tool down into the billet, and up the center of the tube comes your extrusion. It's a question of what's moving: is your press stationary or is your press moving? But you end up with dead zones, and I want to show you some of the defects.

§9.p2

Here's one set of defects, or inhomogeneous deformation. This is a copper cast — you can see the grain structure from the original casting, and they extruded it partway. Pure copper over here; this is 70-30 brass done the same way. Look at the dead zones. Copper has a little dead zone — you can see the grain refinement. This is a reduction ratio of about 85% on both. But look at the shear bands in the brass. The different work hardening between copper and brass gives you a very different pattern and these dead zones. That kind of pure shear not only raises the forces necessary to do the extrusion, but it ends up giving you lousy surface finish coming out of the die, because you're rubbing metal against metal — galling, if you will.

§9.p3

The last thing we'll do is talk about Stamixco, which we were talking about with some people before class. If you're doing polymer extrusion — an injection molding press — it's like a great big toothpaste tube. It might be 30 feet long, made out of steel three inches thick, but it's just a toothpaste tube. You're going to squirt polymer out and extrude it into something. Part of the problem is, a lot of times it's like a two-part epoxy — you want to mix two polymers together. If they're very thick, it's hard to get them mixed well. So this is what they call a static mixer. That's where the name Stamixco comes from. Pretty simple tool, but there's some technology in the design.

§9.p4

You basically have this type of thing that goes into your extruder barrel — goes inline. You've got your pressure ram, your dies and everything up here. The polymer melt, or polymer in a partially molten state, is brought in here, you put it through all this, and you get it to mix. They've taken a blue plastic and a white plastic, brought them in — blue down the center and white on the outside — and put them through these elements. There's a three-dimensional model, and in just a few lengths you've got light blue: it's mixed. If you tried to do that without something to create the turbulence, it would take you half a mile with things of this viscosity. So this is extrusion of viscous polymers. Here's the starting material — blue core, outside tube.

§9.p5

Turns out the guy who runs this company is an MIT chemical engineer, has a PhD, very nice guy. He came to me once — we had done some work on something else — and he'd gotten together with these guys. He'd run a contest at a polymer extrusion conference: here's an extrusion we did with the blue resin in the center, and when we're all done, the blue resin is on the outside. It's not on the inside. How did the blue resin get to the outside? He had a $500 contest for the students. He wanted to run a contest at MIT to see if MIT students could do it, because out of 50 students at the conference, only one young woman figured it out. He was so proud of his thing.

§9.p6

So does anybody have an idea how the blue resin got to the outside?

§9.p7

Student: Diffusion?

§9.p8

Nope, not diffusion. What have we been talking about? Inhomogeneous flow. If you had looked at this thing at some step in between, you'd have found that you had white sticking by friction around the boundary on the wall of the mold, and blue bulging in front. So here's white, and here's blue. Keep doing that for a while, and the nose goes up further and further, until finally the nose folds over on itself and turns 180°. Look at the top here — it folded over up there. If you had seen it at an intermediate stage, you would have seen this stuff bulging — inhomogeneous flow.

§9.p9

He was very disappointed to find that I could solve the problem in five minutes. I didn't give you five minutes because we didn't have five minutes. It's partly because I think in terms of deforming metals. Here's a polymer problem. He's a chemical engineer. In his mind — and if you read some of the stuff, he explains this in terms of a boundary layer, because a chemical engineer or a mechanical engineer understands boundary layers and they think of the world in terms of boundary layers.

§9.p10

I had a problem once which was a problem in current flow through copper and steel when we were doing welding. The steel would go past the Curie temperature and become non-ferromagnetic, and that's going to really affect the way the current flows through the thing. I went to see Jim Melcher, one of the great scientists at MIT, who passed away about 15 years ago. We started talking diffusion. To me, diffusion is: you have a vacancy, an atom moves into the vacancy, and they change places. Jim Melcher started talking diffusion, and he drew me an infinite series of parallel resistors. He thought of everything as an electric circuit. I thought of diffusion in terms of atomistics. Mike Mousakas thinks of the flow in Stamixco as a boundary layer problem. I think of it as inhomogeneous deformation. Even though we're all engineers, we speak different languages. That's one of the lessons for today. I'll see you on Tuesday.

Cases referenced

  • Black Hawk helicopter tail rotor washer failure §1.p2

    Recap from prior session. Tom brings the physical washers (Seahawk and Army variants, both steel and aluminum), explains the saw-cut residual stress measurement method (8 ksi measured), and the resolution: switch from a heat treatment with 5 ksi SCC threshold to an overaged T73 with 25 ksi threshold.

  • Vacuum arc remelting of aerospace steel §2.p4

    Triple vacuum arc remelting as the standard for aircraft crankshafts, landing gear, transmission shafts, and turbine engine shafts. Used to illustrate why inclusion control matters for fatigue-critical components.

  • Bethlehem Steel summer training program (1975) §4.p4

    Tom's first-summer experience at Beth Steel forging plant — 500 new engineers, week of vice-presidential talks, observation of manual oxide-scale removal from large forgings.

  • Japan Steel Works 600-ton upset forging §4.p2

    Visual aid (photograph) showing barreling and oxide breakaway under the gripping tongs. Tom uses it to illustrate friction-induced inhomogeneous deformation and to anchor the practical scale: largest forgings today are about 750 tons.

  • Naval Air Rework Facility jet engine rebuild §6.p4

    Tom's second-summer civil service job during Vietnam war — rebuilding jet engines from crashes. Mentioned as biographical context rather than developed as a case.

  • Al Backofen — biographical anecdotes §6.p2

    Backofen's retirement from MIT in mid-fifties, his $90,000 Marblehead house sale, his New Hampshire Christmas tree farm ($3/foot, ~10,000 trees/year, $50–60K income), and his antique-resale trade between New England yard sales and New York City. Tom's salary comparison: $15,000 as assistant professor.

  • Backofen rediscovery of superplasticity (1965) §5.p3

    Backofen's 1965 rediscovery of German pre-WWII superplasticity work, which enabled isothermal forging of jet engine turbine discs. Tom references graphite and molybdenum dies for hot superplastic forming of nickel superalloys at 2200°F.

  • Nasmyth steam hammer and SS Great Britain propeller shaft §6.p1

    James Nasmyth's painting of his patented steam hammer forging a 30-inch wrought-iron propeller shaft for Brunel's SS Great Britain. Tom uses the V-shaped anvil visible in the painting to make a delta/triaxial-stress point.

  • Amtrak Acela trolley wire — Phelps Dodge vs. Rome NY supplier §7.p1

    Full development as the lecture's lead applied case. Tom's December consulting trip to Rome, NY; rejection of $4.5M product on December 23rd; arbitration in Old Saybrook, CT; FBI raid on the British supplier company; the elongation-spec upper bound (8–14% required, Phelps Dodge product was 18%); the orange-peel-effect mechanism revealed by Providence test-track sparking video.

  • Tony Thompson doctoral thesis on grain size and fatigue in copper §8.p9

    Cited as the literature Tom drew on to justify the Acela trolley wire rejection. Thompson was Backofen's student and Tom's first lab supervisor at MIT.

  • Eagar wire-drawing thesis (superconducting wire) §7.p6

    Tom's undergraduate thesis: $1,000 worth of diamond dies bought in 5% increments, which Tom now identifies as the wrong approach — should have used 30–50% draws to avoid high-delta operations and centerline cracking.

  • Jim Melcher diffusion-as-circuit anecdote §9.p10

    Tom's welding/copper-steel current flow problem with the Curie transition; Melcher (MIT) drew an infinite series of parallel resistors instead of thinking atomistically. Used to make the lecture's closing point that engineers from different disciplines speak different languages.

  • Stamixco static polymer mixer puzzle §9.p3

    Mike Mousakas's $500 student-contest puzzle: blue resin starts in the center of an extrusion and ends up on the outside. Mousakas (chemical engineer) explained it as a boundary-layer problem; Tom solved it in five minutes as inhomogeneous flow (white sticks to the wall, blue noses forward and folds over). Used to close the lecture on the theme that engineers from different disciplines describe the same phenomenon in different vocabularies. ## Figures referenced (recurring numeric anchors)

Layer 2 — cleanup edit
p1 00:04

Um in any case, the first thing which I may have to remind people: Tuesday, I'm going to give you Monday off, you can have Monday as a holiday, but then Tuesday is actually Monday at MIT. This is, we do this once every spring term. The people who schedule things want to have the right number of Mondays — Monday-Wednesday-Friday classes — and the right number of Tuesday-Thursdays, and the way they do this in the spring, they always have to turn a Tuesday into a Monday. So next week I'll be lecturing Monday — or Tuesday — and Wednesday, which will both be in this room at 9 o'clock. Okay, so if you go to 26-100 at 11:00, have fun. Uh, and you can watch the video later, and actually you're getting the videos up within a day or two now, right? They should be going up pretty quickly. Yeah, every couple days. We had some problems earlier this week but I think it's all resolved, so they should be going up fairly quickly. Anyway, so Monday — or Tuesday — and Wednesday I will be lecturing in here at 9:00. Simone will be doing both Thursday and Friday of next week, okay, as far as that goes. So we've taken care of that.

p2 01:09

Um, we talked about the Blackhawk U-washer yesterday — or two days ago — and so I actually brought a couple of my little pieces left over from fifteen years ago. [Tom produces the washers.] This is actually the washer, and fifteen years ago it cost $350. This one's painted gray; actually that means it's a Seahawk. This one's green, this would be an army part. This one's steel, this one's aluminum, don't ask me why. It's actually a very clever design. In order to keep it tight, there's a different number of holes in this than there are in here, and so no matter how you turn it, within about two or three degrees you always get one hole to line up, and so they put a screw in there to keep the thing from loosening. They don't use lock wire or anything, friction or anything; they actually have a positive thing, because if you lose your tail rotor you just spin to the ground, which is exactly what happened.

p3 02:10

But the reason they lost their tail rotor is this washer. In the incident, one developed a stress corrosion crack. I don't know if it developed it there, but we actually took this one which had never been used — the reason there's a saw cut there, we measured that, there's some flats here that keep this thing from rotating, and we measured the distance very precisely, you know, within a fraction of a thousandth of an inch, and then we made the saw cut and we measured the distance, and depending on whether it shrinks or opens you can calculate from this — it's basically just a simple circular beam — and you can calculate how much stress it took to open it or close it. We found 8 ksi. We measured 8 ksi residual stresses in this part, and it turns out with the type of heat treatment for the alloy it's made out of, 5 ksi would cause stress corrosion cracking. And the solution was to go to an overaged T73 heat treatment which has a stress corrosion cracking minimum of 25 ksi. So they had been making it out of something that was only good for 5 ksi stress corrosion cracking resistance; they later switched to 25 ksi material, which is just a heat treatment change, it's not a compositional change. And then the residual stresses were 8 ksi, so everything fit together in terms of explaining it. So that's just filling in on that.

p4 03:38

Now, a question — I kind of said, oh gee, I wish I had brought Backofen with me, but fortunately they didn't erase my wonderful drawing over here. We were talking about necking and void formation in a tensile test, and that's what these are, graphs out of Backofen. So you're doing a simple uniaxial tensile pull, and here's the fractured specimen, here's necking. If you actually look — in this case, a piece of copper — you actually find in the neck, if you cross-section and do metallography, you actually find a bunch of voids that are forming in the neck, okay. The neck goes on into a state of triaxial stress. Okay, we'll talk about stress states later, but it's basically being — it goes into a hydrostatic tension, if you will, and that's what's helping the voids open up. The whole thing's being pulled in all three directions. If you look at a higher magnification, you actually see these elongated voids, and you actually can see some copper oxide particles — these little black spots are inclusions, copper oxide inclusions — and in the holes they're actually acting to nucleate something. This is all — oh, it's 9:06, this can be official now.

p5 05:00

Um, this is, I think, out of Hosford. This may be in your book. Hosford has some pictures and you actually can see the fracture in the neck, what we call ductile dimple rupture. This is a cross-section, and you can kind of see the cross-section of the dimples and how the voids are forming, pulling apart. Classically, people will say, well, this is looking down on the fracture in the scanning electron microscope, and you see the ductile dimples like taffy pull at 1,000x, okay — 3,000x, okay, sorry — actually it's even bigger than that on the screen, but anyway. Inside many of these you'll see the oxide inclusions that are nucleating each dimple, okay. So that's classic ductile rupture. I've now preempted Dr. Belmar on ductile fracture, anyway.

p6 05:54

So these things do sort of fit together. Backofen has this drawing: if I had something with no inclusions and it was just a nice, very clean material and I pulled on it, it might neck down like this. I get tremendous elongation. If I had something that was — and you do just a thought experiment — that the inclusions basically break this thing up into a bunch of fibers, if you will, okay, smaller tensile specimens, and when they neck down it's like necking down a bunch of fibers, and now the total elongation with inclusions is a lot less than the elongation if the material was very pure. And in fact that's true. We know that's true. Uh, back in the '60s and '70s, we spent billions of dollars coming up with vacuum arc melting and all these fancy things to get rid of inclusions in metals because they are crack starters.

p7 07:00

In fact, all the crankshafts and all the piston engines and aircrafts have to be triple vacuum arc melted now, because vacuum arc melting essentially burns away the inclusions that formed from the regular steelmaking process. So they make the steel, cast it into an ingot, and then they take this great big ingot and do it — and they arc it into another mold. So you got a round ingot that you cast, it's got full of dirt and inclusions, and then you basically arc it into a copper mold, and you withdraw the mold and you just remelt it, but it's in a vacuum. So now in the heat of those little pieces, little spatter of metal going across there, they're being melted in a vacuum now, and it sucks out the oxygen and the nitrogen, and you end up with a very clean steel. They will triple vacuum arc remelt aircraft landing gear, transmission shafts, the shafts for turbine engines. I mean, they're using steel for these things and they're triple vacuum arc melting them to get rid of the inclusions — once, twice, and three times. And you're actually getting things that are so clean that you look at them at 500x and you have a hard time finding an inclusion in the microscope at 500x. And there's standards for all these inclusion counts and things like that.

p8 08:24

So then, someone — one of you brought up, or asked me something about — and I said, yeah, we call it orange peel. Here's a picture of orange peel. I think this comes out of Hosford's book too, probably chapter 16. This is — I don't know what it is, looks like it might have been a gas tank, the bottom of a gas tank or something in the automotive industry, but it's a drawing from a stamping from sheet metal, and the surface looks like an orange, right? I told you it did, right? There it is, looks like an orange. Um, it's caused by large grain size. Those little pebble surfaces, each one of those is actually about the size of the grain size in the material. If you want to avoid this type of imperfection — I'm not going to call it a defect because it really doesn't weaken the material, but it does, if you wanted a nice fender on a car, it wouldn't be very good, okay, the paint wouldn't cover it up. So it's not generally desirable. You have to control the grain size, and we'll talk about that at a later time.

p9 09:34

Um, the other thing I wanted to do, is I could tell on Monday, going back several days, I was talking about redundant deformation, and how — I guess I don't have it, I can find it — but anyway, how you look at the deformation zone geometry, and if you're at a delta of one and it's just sheet rolling or something like that, everything kind of straight-line deformation, they had kind of x's in there. But if you get to a delta of four or ten, the slip lines all have this curvature to them, and I tried to say, when the slip lines are straight, you have uniform deformation, it's homogeneous deformation. When they start to curve at higher delta, you have non-uniform deformation, you get inhomogeneous straining, it's redundant deformation. And the redundant deformation comes from the fact that you actually have to bend it one way and then bend it another way and then bend it another way. And I kind of said that, and some of the eyes were glazing over at that point.

p10 10:35

So here's my example: two decks of cards held together with rubber bands. [Tom produces two decks of cards.] If I deform it, I shear. Remember, the plastic deformation only occurs in shear. Hydrostatic compression or hydrostatic tension has no effect on deforming the metal. It might allow it to go out to a higher elongation, but it doesn't cause the shape change. The shape change is due to shear. So if I do a shear on this, there's, something at a delta is equal to one, type of shear. At delta is equal to five, you basically shear it that way, you shear it back the other way, and then you shear it that way to get the same shape change as delta is equal to one. You did three times the work to get to the same thermodynamic state, okay. Remember, in thermodynamics, the end states are state properties, and they tell you the energy or the shape of the material in this case, but they don't tell you the path. And the path — it's not — the work is not a path-independent property. It's — work is not conserved. And the work — the shear work to go this way, back that way, and then this way again — I get one shape change for three, but I pay the price three times in terms of energy, right? That's redundant deformation. That redundant deformation leads to inhomogeneous flow, okay. And a lot of that inhomogeneous flow comes from friction.

p11 12:07

Okay, so this is out of Backofen, and this basically shows you delta dependence of inhomogeneity factor for copper strip with different types of lubrication. So here's delta, and this is basically copper strip where, you know, you got something — delta is equal to one is the height and the width of the deformation zone are equal, right? Here you're really in a rolling situation; over here you're starting to get to something a little more towards drawing or extrusion. In any case, you can change the die angle of the draw. Anyway, unlubricated, the inhomogeneity factor as you get to higher and higher delta increases. And we saw that in that little handout that I just gave you — passed out — when we went through and we saw the different delta operations, the inhomogeneity factor increases when you have less die angle, okay. And then if you got paraffin oil or soap — and remember, soap, those are the stearates, and later we'll talk about why stearates are such good lubricants.

p12 13:20

Okay, we also can talk about why, if you live in an area with hard water and you take a shower, you still feel soapy even though you've rinsed off. Does anybody know about that? Anybody live in an area of hard water like San Antonio? You lived where? New Jersey. Okay, if you have a lot of calcium in your water, that's what's called hard water. In fact, the amount of calcium in the water is called the hardness, okay. And there's soft water, like New England has nice soft water. Take a shower in New England, rinse off, you feel nice, and you don't feel slimy and soapy. But in San Antonio or certain parts of New Jersey, they probably are using groundwater, not rainwater, but they're probably using well water in that part of New Jersey. Okay, duh, how did I know that? Because it gets saturated with limestone and it gets a lot of calcium. And what happens is, the soap is a calcium stearate, and if your water is already saturated with calcium, you can't dissolve off the soap. A monolayer of soap molecules, of stearate molecules, stays on your skin, and you can rinse till the cows come home and you're still going to feel slimy when you get out of that shower, right? I mean, I travel around the country and go to a hotel, take my shower, and I can tell you what the hardness is of the water — not exactly, but I can tell you whether it's hard or soft water. San Antonio has hard water, um, but I know that for other reasons, okay.

p13 14:57

Any questions? So now we want to talk about sort of forging type of deformations. This is almost a delta one, not exactly one but close to one. Uh, not everybody uses delta, okay. Backofen liked to use it, and his students Hosford and some others like to use it, but you go back before the 1960s and most people don't talk about delta operations in terms of deformation. In any case, this is showing two different friction levels in metal flow. You start with something that looks like this, you reduce it 8%, 22%, 33%, 44%, and 60%, and you can see the inhomogeneous deformation, okay. The rectangle has turned into — the squares in this rectangle turn into, in the center maybe they're still squares, but out the edges they got funny shapes. And as you go further and further, you get worse and worse in terms of the uniformity of your deformation.

p14 16:02

Um, this type of shape change, this would be a frictionless type of deformation, but you typically have something that causes this barrel shape. See, intermediate in here, you can see why I call it the barrel shape. If you want to see the barrel shape in the real world, you can go to — this is Japan Steel Works, doing upset forging of some big heavy something or other. I can get it on here, let me see — try to do it. I was looking for this book yesterday and couldn't find it. Anyway, I had it on my cart, couldn't find it on my shelf. Anyway, so here's upset forging of big hot piece of steel and you can see it's starting to barrel, okay.

p15 16:57

Um, this thing's pretty big. This is a 600-ton forging, okay. The largest forgings we do, or the largest pieces of steel we do, are about 750 tons, so they don't get much bigger than this. Uh, anybody have an idea why it looks kind of whitish right underneath the clamp? [Pause for student response.] Because we broke off the oxide. In order to heat this all the way through, you had to leave it in the furnace for a week, and you leaving it in a furnace — it's just an air furnace at about 2200°F — and the iron oxidizes in the furnace, and the oxide's about an inch or two thick, okay, after a week at 2200°F. And now you grab it with these big tweezers — they're big tweezers to pick up a 600-ton piece — and the oxide breaks off. The oxide has a different emissivity. I mean, it's not important, but when you actually forge this, you will have this hot slag of oxide, it'll all break off.

p16 18:01

And I remember the first time when I worked for Bethlehem Steel during the summer, they had a little program to introduce all the 500 new engineers that year to steelmaking. And in the morning, we would listen to vice presidents give talks. This lasted for a week, and that tells you how many vice presidents they had in this company, that you could spend five mornings listening to the vice president. It wasn't — they weren't long talks. I mean, these guys had a half an hour each. Um, and then in the afternoon we'd actually go down to the Bethlehem plant. And I remember going to the forging plant, and they had great big forging presses like that, and this was 1975 — summer of 1975. And they had a big forging hammer slamming down on these things, and when the great big crane moved the steel back and they were done, two guys, two bare-shirted steelworkers, went out there with their shovels scooping up all the slag, the oxide that had come off the forging. I mean, it was only about six inches deep there on the forging bed, you had to scoop it off, because if you brought another one in, all you do is forge all that stuff into the surface of the next one you're going to do.

p17 19:19

So they had — it was all done manually with these guys, and it was amazing to me. I sat there kind of bug-eyed. They had a dumpster that they had brought up, and one guy would scoop, he'd go down to scoop, and the other guy — and then he would come up and throw it over his shoulder into the dumpster of this hot slag at about 1,000°F, okay. The other guy would go down, and they were like pistons going back and forth. And I thought — I said to a guy, I said, what if one of them got out of sync and threw hot slag in the other guy's face? And the guy says, well, they've been doing it for thirty years. And the guys who do throw it in the other guy's face, they probably don't work there anymore because they may be dead, okay.

p18 20:12

But the die starts out cold, and by the time you end up forging, the anvil, which may only be four feet thick, okay, and the hammer above, which may be another two or three feet thick — you don't want to touch it, it's probably pretty warm, it might get up to 1,000°. You're forging something at 2200, and you're hammering it. I mean, go watch the blacksmith here in the basement, okay. You know, he starts out with a cold hammer and he hits something hard, and when he's done, that hammer gets warm. But it only gets to about half the temperature of the thing you're forging. Now, if you keep on hitting with that same hammer and don't let it cool off, then you're going to have a problem, because it heats up, and now you're hitting — what you're doing is, you're taking one material that's softened by heat and another material that's strong by low temperature, and you're using the hard material, the cold material, to form the hot material.

p19 21:16

And that's actually something I was going to talk about next week. There's three ways we can form things. We either start with something that's really hard and form something really soft, and remember those little machine screw things — that's cold heading. That's all at room temperature, no temperature effect to give me a strength difference. What do I do there? I heat-treat the steel to 200 ksi strength, and the workpiece is going to be 30 ksi annealed steel, soft as I can get the steel. But as I'm working, it gets up, and that final part is probably 100 ksi, but the tool is still 200 ksi, okay. I got to have some good lubrication. So that's a case of same temperature but I'm using big strength differences to give me my advantage. Then I can use temperature as the advantage, but now I have this process that's not isothermal. I have to have a cold tool in a hot workpiece, and now I have to have a little time in between my working for the tool to cool off, right? And that's kind of your question, yeah, it gets hot, okay.

p20 22:27

And the third one, which we'll talk about, is called isothermal forging, and it was developed because of Al Backofen and superplasticity in 1965, when he rediscovered it from Germany. That's Tuesday's lecture, okay, I don't think we'll get to that today. Isothermal forging is how we make a lot of the turbine discs for airplanes, jet engines and stuff. But it basically is — I mean that's, that sample should be in the Smithsonian. I recovered it from the graduate student's desk; they were using it as an ashtray, okay. Student: Will they just let the forming tool — or they try to cool it? Tom: No, actually, in superplastic forming you get material that, instead of taking a 30% stretch, will take a 400% stretch. So you come in with — sometimes you can use graphite dies, okay, which are not particularly strong, but you get the material up to where it's like clay, okay. You take the superalloy, the nickel-base superalloy, up to 2200°F, and it will deform like clay. But you have to have something that's a little stronger, but it can be something that's relatively weak, like graphite dies. You can use molybdenum dies, you can use other superalloys which have a little bit more temperature, okay. The die materials, you're limited in your die materials, but everything is hot, it's isothermal. The dies are just as hot as the workpiece, and you're using something that's a little bit stronger but you're using a material that's superplastic, okay.

p21 24:10

In isothermal forging — we'll talk about it next time, I have to explain how you get superplasticity first, okay — but it's, we could not build the jet engines that you fly on. When you fly on, you know, United or Delta or American or whatever, uh, you're flying in a whole different technology than in 1960 when I flew up here to come to school as a freshman, okay. It might have been jet engines, but boy they're a lot different, okay.

p22 24:44

Um, now I did want to show you one other thing in here. I actually had a lot of things that I could show you in here. That's — but the one I really want to show you is this one, okay. This is James Nasmyth's painting of his patented steam hammer forging the propeller shafts. This is a 30-inch diameter shaft for some Middle Eastern kingdoms — Brunel's, okay. Is Brunel in the Middle East? I think it was Middle East — anyway, they were building a ship called the SS Great Britain, it was going to be one of the largest ships. These were the largest wrought-iron forgings of their day. It was just a steam hammer, big steam cylinder up here, just a hammer, and they're going to take some ingot of wrought iron. This isn't even steel technology, this is wrought iron technology. Look at the manipulator they have back here. Count them, okay, there's actually men moving this thing. You got an anvil right here. Notice the shape of that anvil, it's V-shaped. Remember, I showed you the picture of how you don't want to do deformation at delta is equal to 5, of just two platens coming together, because you'll crack the inside, it goes into tension. But if you do it from three sides, use a V-shaped anvil, you will actually get compression in the center, you can drive the center into compression and not cause splits in the center. 1839 — they had studied Backofen, they knew all about delta, and that's why they were using their V-shaped anvils, right? Just want you to know, it all, you know.

p23 26:23

Someday I have to tell you some stories on Al Backofen. He was an interesting guy. Actually, I'll tell you one of them right now. Um, I'll tell you a couple of them right now. So when I came back when I was a sophomore, I had worked 240-hour-week jobs that summer between freshman and sophomore year. I'll tell you even more — it was like during the Vietnam war, and I was lucky enough — I took a test to get a summer job, I grew up in Virginia Beach, Virginia, to get a summer job. And I scored high enough on the test — this is not the hardest test in the world, it's the civil service test, and you had to be able to add two and three, you know, rather than just two and two, I mean, really hard questions — and I got above a 95. I may have gotten a 98 or a 99, but that was high enough that I got hired as a postman.

p24 27:17

And the job I had the summer before, I got paid a dollar an hour as a clerk down at the Beach in Virginia Beach, a clerk in a drugstore. Well, the post office paid me $3.35 an hour, okay, that was a standard rate. And I was basically replacing postmen who were going on vacation for two weeks during the summer. They hired a bunch of subs, and I did all kinds of jobs. My favorite part of it — into the summer, they had me delivering special delivery letters, which is like express mail today. This was before FedEx, and for 35 cents you could pay to get the letter delivered special delivery. And so typically I would show up at 9:00 in the morning, they would give me ten or twelve special delivery letters that had to be delivered immediately in Virginia Beach. So I'd get in the station wagon, and I would drive for the next eight hours, because Virginia Beach at the time was the fifth-largest city of the United States by area, okay. We don't have to get into the reason for that. Chesapeake, Virginia, was the third-largest, okay, by area. They had incorporated whole counties under Virginia law into cities so that Norfolk wouldn't and Portsmouth wouldn't annex them. But anyway, I just did tell you the story. Anyway, so they're paying me 24 — a little over 24 bucks — to deliver $3 worth of mail, right? And we wonder why the post office is going broke, okay. They've had this model of service-with-a-smile and at one-tenth the cost for years, okay, it goes back a way.

p25 28:58

So anyway, the next summer I needed to make my three bucks an hour to pay my MIT tuition and all this other stuff, so I did the civil service thing again. They hired me at the Naval Air Rework Facility, where they rebuilt jet engines, and we got all these crashes coming back from Vietnam and we'd have to rebuild the engines. And I was just an engineering trainee and stuff, but then — that was only two bucks an hour, I needed to make that extra buck an hour, so I took my old clerk job back at a buck an hour, and I worked 80 hours a week at two jobs 30 miles apart, and it was not a great summer, okay. So I came back here, and I decided I would work in the lab.

p26 29:34

And I went — I'd taken my mechanics of materials class, my first materials course other than 3.091, Al Backofen is the professor, and I went up to him at the end of the class. I said, uh, professor, would you have any jobs in your lab that I could do? And he says, well, come back to me next week, and I'll let you know. Well, he came to me at the next class. He says, I found a job for you, go see Tony Thompson. So I started working for Backofen, and he was a very kind man as long as you weren't his doctoral student. Um, if you're a bachelor student or a master's student, he was just a gracious gentleman. White hair, always wore a bow tie, okay, kind of bow-tie academic, looked like an academic with his tweed sport coat and stuff. And anyway, so when I started, they put me in that little short door, 8-137, that was my office. It was Backofen's graduate students'.

p27 30:28

Backofen was leaving the week that I came. He had retired in his mid-fifties. He couldn't get along with anybody, he decided, to heck with it. And um, he was leaving MIT, and uh, I was starting. But he always had kind of had a, you know — he had liked me, I'd been one of his undergraduates, and he came to me, he knew I was starting, and he gave me a piece of advice, and the piece of advice is: the only way to keep your sanity around here is with a pocket full of Valium, okay. I've always remembered that.

p28 31:06

And he went off — um, he had a home up in Marblehead. Now you got to remember, this is 1976, um, and he and his wife decided they would put it on the market for an outrageous price: $90,000. And if anyone offered it to them, they would just move to New Hampshire, to their farm in New Hampshire. Well, the first person who came by offered him $90,000. He obviously didn't have a clue what this place was worth, and he sold it, moved to New Hampshire. And about twice a year he would come back when I was an assistant professor, and he'd always stop by to see me, okay, and ask me how I was doing, okay, and I would ask him how he was doing. Well, in his later years — he only passed away about two years ago in his eighties — he had started a tree farm, a Christmas tree farm in New Hampshire. This was before you could buy nice pruned Christmas trees, and he would go out there in the spring and he would spend his time out there pruning the trees. And he would sell those trees for $3 a foot. So if you want to buy a 7-foot tree, it's like $21. Well, 1970 — I mean, this is, ordinarily you'd be paying $3 for a Christmas tree, and it'd be all this scrawny — he was leading the market. Nowadays you get all these pruned trees, everybody prunes trees, but he was one of the first ones. He was selling 10,000 trees a year and making about 50 or $60,000. My salary was $15,000 as an assistant professor, okay.

p29 32:32

The other thing he would do up in New Hampshire and Vermont and Maine, is he would go out and he would go to the yard sales and buy the junk, and then he would take it to New York City and would sell it as antiques. So what one man's junk is another man's treasure, okay. And he told me he was making more money than he had ever made as a consultant or a professor, okay. So Backofen was a — he was a character, okay. Anyway, maybe someone will tell a story about me being a character someday. Might, anyway.

p30 33:06

Um, so I want to start showing you some of the types of flow you get from inhomogeneous deformation. Here's a forging, hot upsetting of steel with sticking friction. Well, sticking friction means the stuff under the tool doesn't move at all. The material is stuck to the workpiece, and all you have to do is not put the glass lubricant. Typical lubricant for hot forging — well, steel forging, like I showed you, you don't use any lubricant, you just let the slag fall off, okay, the oxide scale fall off. But if you're doing a nickel-based superalloy or something, you actually encase the whole thing in a glass frit, and when you get it up hot, you now have this syrupy layer of glass, because the glass melts and gets thick, and if you pick the right glass that it's at the right forging temperature, it'll be a good lubricant.

p31 34:00

Anyway, so this is one they did without any lubricant, and you can see the material flow lines. Initially, this material right underneath the tool didn't deform at all. This material might as well have been a part of the tool. That stuff, the flow lines — it was like you can think of it as grains of wood in the original billet of steel, and it just shrunk around. Like here, bowed out, but notice how it's now curling around, and you're going to form a defect. If you kept this thing going, you're going to get a little lap, okay. So that's the effect of friction, and you can see the inhomogeneous deformation. This material didn't get worked at all. This material got, you know, this direction, that direction a number of times, okay. So that's where inhomogeneous deformation comes from.

p32 34:55

Let me give you another example. Uh, this probably comes out of Metal Forming by Altan. But this is a titanium blank, which is actually an alpha and beta microstructure initially, and it's been squeezed down, and the microstructure afterwards from the etching, you can see, looks like it's fairly uniform — little barreling at the ends — but it flowed fairly uniformly. This is an all-beta microstructure. Titanium comes in alpha form and beta form. Alpha is hexagonal close-packed, beta is body-centered cubic. If you try to forge something in the alpha-beta range, good deal, okay, nice uniform product. You try to form it in the all-beta, look what happens. You get shear bands, localized shearing. And all this other material — you got the big coarse microstructure, and then you got these bands here in between. See, you see the X from the delta's-equal-one type of deformation. Basically, the stuff's tried to shear on these simple little X-planes. The X kind of got distorted, but see the X? Okay, those are the shear bands.

p33 36:05

Um, now let's look — this comes out of, well, this might come out of Hosford. So one of the things people do, they actually take modeling clay. I'm not kidding. They take modeling clay — now they do it, they do a finite element analysis in the computer, but in the old days they would take modeling clay, they would put two pieces together with nice flat surfaces, they'd scribe grids on them, and then they would extrude the two pieces through the same die, then pull it apart, and you could see the flow lines from these things they started with. And here we have different die angles, okay: 40, 45, 60, another thing with a different angle. And this is actually Don Blickwede again, my old boss when he was vice president of Beth Steel, okay. Those actually may be steel billets rather than clay, but anyway, cold-extruded billets, okay.

p34 37:03

But if you start looking — this is someone else's data — but if you look at the hardness number — so they're now looking at hardness and different amounts of deformation, the distance from the center. So you're looking at hardness across something like one of these billets, and with zero deformation of course it's uniform, everything's nice little squares, and of course with zero deformation you have low hardness number. If it's steel, let's say that's a Rockwell B 50, something — very annealed steel. And as you go up in deformation from 4 to 6 to 13 to 26, you'll see that initially you get very inhomogeneous deformation across there based on the hardness numbers. You get a lot of deformation, and everything becomes homogeneous again because it's all fully kneaded, okay. You've really beaten down that pizza dough. So if you're going to make a pizza, it's going to have a uniform crust. This is the practical things in this course. You've got to knead it a reasonable amount. You don't do something in between, okay. If you do nothing, you don't have much. The first stuff introduces a lot of inhomogeneity, and you really got to get to 40% deformation — that's 40% stretch — is a fair amount of stretch before things start to get homogeneous again, okay.

p35 38:28

So I used to think, when I was a bachelor student here, and I was doing wire drawing for my thesis to make superconducting wires, that I would do better if I would do — I had a great big set of wire dies, okay, you could buy diamond dies for 20 bucks a piece back then. So I had a government research contract, I went out and bought $1,000 worth of dies, and I had them in 5% increments, okay. Well, that was the wrong way to go. You really should be doing 30 or 40 or 50% draws, and not 5 or 10% draws, because with 5 or 10% draws you get lousy deltas, okay. You get a high-delta operation, and you're allowed to crack the center, okay. And you also are going to get very inhomogeneous deformation when you do high delta. This is a very — this is the highest delta operation among these four, okay.

p36 39:28

Um, but in any case, so that's one thing to remember, that if you're going to work it, you got to work it a lot. And I guess I do have another story on that, um, so we still got time. You know, I never know what story I'm going to tell. It's just a question — I mean, I think about it ahead of time, believe it or not. So here's the trolley wire again, okay. [Tom holds up the trolley wire sample.] So there's the trolley wire. This trolley wire has got an equivalent delta of about 30, okay. Super-fine grain, it actually is starting to get to the region, I believe, of superplastic. Made by Phelps Dodge.

p37 40:14

But the company that originally had bid on this — um, this was for the Northeast extension of Amtrak, the Acela line from New Haven to Boston. There's a $330 million federal contract to build this line, and that was the product they wanted to do. They had to purchase somewhere between $4 million and $7 million worth of copper to mount it. And I get a call about — I think like December 20th, 21st — saying, uh, Tom, can you go to Rome, New York? There's a little company that's making our trolley wire. This is from Amtrak, the Amtrak engineer. And you go to Rome, New York. So we drive out there on the 22nd, and they say, oh, by the way, we need an answer before Christmas. That's not very far away from December 22nd.

p38 41:06

But what they had is, this company had been making the largest wire — they had been making copper wire for years, but the largest diameter they had ever made was 5/16 of an inch. That's over half an inch equivalent, okay. They had never made anything much above a quarter of an inch in diameter. And the largest mold they had, a continuous caster, this was the size of the largest mold — it's like an inch and three-eighths or something — and you can see the grains, okay. There's a longitudinal cut and another cut. Huge grains. Remember I showed you earlier, I showed you the orange peel and stuff. If you have large grains and you deform something — and Amtrak's question was, are we going to have problems with this large grain size, because the company said, well, we're meeting your spec, except we don't have small grains, is that okay? That was the question. And so I'm supposed to give the answer before Christmas, okay, by going out there and looking at this.

p39 42:09

Well, it turns out I told them on the 23rd to reject the product, $4.5 million worth of product, okay. Uh, well, turns out it was a fixed-fee-price contract with the US government, and the company had certified to the US government that this company in Rome, New York, that had never made wire bigger than 5/16 of an inch, was the only company in the entire world that could make this trolley wire. Okay, because Amtrak had some very tight specs. This is a copper-silver alloy, it had to have a certain amount of elongation, you know, when it's — anyway, so, mechanical properties. And so I didn't realize all this stuff, but I had rejected it. Uh, I told the Amtrak to reject it, so they sent a letter saying we reject it, you can't put this up, you have to go find other material. But they had already certified there was no one in the world that could make it to the Amtrak specs.

p40 43:06

Well, it turns so happens that Phelps Dodge, the second-largest copper company in the world, had been begging this company for two years to make a bid on this. And the problem was, their alloy was so good and had all this redundant deformation and super-fine grain size that it had — Amtrak for some reason had a spec of between 8 and 14% elongation, and this stuff had 18% elongation. It had too much elongation. It was too ductile. It was too good. It was outside — why someone said the elongation should be between 8, gave an upper limit. Ordinarily, the elongation, there's just, you have to meet a minimum, right? And this company had not allowed Phelps Dodge to make a bid because they exceeded the maximum, when there should have been no maximum, okay. But that's how they had written the spec, and so technically, they wouldn't let them bid, even though it was going to be a much better product, okay. And actually, you can see, I mean, I got some — you've seen the tensile bars, I sent them around, they neck down, you know, big stretch, right?

p41 44:17

Um, well, um, what it really matter — it turns out Phelps Dodge price was going to be 6.5 million or 7 million, and this company in Rome was going to be 4.5 million, and so the money in the pocket of this British company was going to be an extra 2 and a half million of profit if they could convince the government to buy this junk, okay. Their junk, okay. But I had rejected it, so it goes to a one-week-long arbitration down in December at an ocean resort in Old Saybrook, Connecticut.

p42 44:51

Anyway, there's a lot — this thing goes on forever — but the bottom line was, when they gave the arbiters the briefings, the attorneys gave the briefings, um, the British company was arguing how Tom Eagar was just absolutely insane and incompetent metallurgist to have rejected this material. He had no basis to do it, and it cost us $2.5 million and the government owes us $25 million extra because they forced us to go out and buy the Phelps Dodge material. Well, okay. The briefing from the government was: you committed fraud on the federal government. You told us that there was no one else willing to bid on this in the entire world, and we found out that Phelps Dodge has been trying to bid on this. And so the attorneys from the British company realized, oo, we could be sued criminally. And in fact, that's exactly what happened a week after the arbitration. The FBI raided the offices of the British company, took the passports of the senior managers, took their computers. And at that point I was out of it, because, okay.

p43 46:02

Um, but, don't defraud the federal government. That's one of the — I mean, Amtrak has the legal authority to put you in jail if you tell them a lie, okay. Now, other companies, they tell lies to each other all the time, but it's not good to do it to the federal government, they can do things. Um, the other part of that story was, the way we actually won with the arbitration — there really was nothing in the literature that said you couldn't do this, okay, that the grain size should be a big problem up there. But it turned out it was essentially an orange peel effect, a large grain size effect.

p44 46:36

Even though Amtrak had told this company, don't you dare install any of that wire, they took about a 10-mile stretch down here in Providence, and they installed the stuff from Rome, New York, and they ran the train along that 10 miles and they videotaped it. And the pantograph, which is the carbon brushes that are running along there — it turns out there was a rough surface on that wire, and as the thing's going along at 60 mph, it looked like the 4th of July. This thing was sparking all over everywhere. If they had put that up for a couple hundred miles, they would have had to take it down two weeks later, because it would have just eaten itself to pieces from all the electric sparks. And the idiots were smart enough to videotape it for us. So, well, you know, but you never said that at the time. Fact is, I didn't know that was the reason to reject it. I did actually look at some data — and this guy Tony Thompson that I first worked with, Backofen, he'd done his doctoral thesis on grain size effects of fatigue in copper, and I went back to some of Tony's papers and stuff, okay. But anyway, um, so there's another little story of, uh, how I got myself in trouble, okay.

p45 47:54

Um, sometimes you just have to make a decision, you know, and sometimes you're going to end up — I wasn't sued directly, but Amtrak was sued for $25 million because of my decision, but we ended up proving ourselves right because they provided the evidence for us idiots. And then, uh, the bottom line was, they — I don't know what happened to the criminal proceeding. Anyway, um.

p46 48:19

Anyway, this is extrusion, and if you go with just straight-edged extrusion dies — and you can have different types of things going on, but in fact you end up with dead zones. And I'm going to show you some of those dead zones in a little bit. This is what they call backward extrusion. You actually push a tube tool down into the billet, and up the center of the tube comes your extrusion. So it's a question of what's moving — is your press stationary or is your press moving? But you end up getting dead zones, and I want to show you some of those defects.

p47 48:50

Well, here's one of the sets of defects, or inhomogeneous deformation. This is copper, this is a copper cast, and you can see the grain structure from the original casting, and they extruded it partway. And pure copper over here — this is 70-30 brass done the same thing. Look at the dead zones. Copper has a little dead zone, you can see the grain refinement. Now, this is a reduction ratio — if this is axisymmetric, which it probably is, it says a billet, so it probably is — this is a reduction ratio of about 85% on both of, well, not both of these but anyway. But look at the shear bands in the brass, okay. So the different work hardening between copper and brass gives you a very different pattern, and gives you these dead zones. And, you know, that type of pure shear, it not only does it raise the forces necessary to do the extrusion, but it also ends up giving you lousy surface finish coming out of that die, okay, because you're rubbing metal against metal, it's galling, if you will, gives you a lousy surface finish.

p48 49:59

Um, now, so the last thing we'll do is, we'll talk about Stamixco, which we were talking about with some people a little bit before. So this is — if you're doing polymer extrusion, so you got an injection molding press, so it's like a great big toothpaste tube. Now, it might be 30 feet long and stuff, made out of steel that's 3 inches thick, but it's just a toothpaste tube. You're going to squirt polymer out of this and extrude it into something. Well, part of the problem is, a lot of times it's like, as you said earlier, it's like a two-part epoxy, you want to mix two polymers together. And if they're very thick, it's hard to get them mixed well, okay. So this is what they call a static mixer. That's where the name Stamixco comes from. And, um, pretty simple tool, but there's some technology goes into the design, believe it or not.

p49 51:01

And you basically have this type of thing that goes into your extruder barrels, or you know, goes inline. You got your pressure ram and then you got your dies and everything up here. But the polymer melts, or polymer materials in a partially molten state, are going to be brought in here, and you put it through all this, and you get it to mix. And so here they've taken kind of a blue plastic and a white plastic, and they're being brought in — you got blue down the center and white on the outside — and you go through these things. There's a three-dimensional model, and in just a few lengths, you got, you know, light blue, it's mixed. If you tried to do that without something to create the turbulence in there, it would take you a half a mile, okay, with things of this viscosity. So this is extrusion of viscous polymers, and it's got all kinds of — here's the kind of starting material, a blue core, outside tube.

p50 52:15

And so, turns out this guy who's an MIT chemical engineer, he's got a PhD, nice guy, very nice guy, he came to me once. We had done some work on something else, and he came to me, he'd gotten together with these guys, and he actually had run this as a test for students at some polymer extrusion conference, and said, here's an extrusion we did with the blue resin in the center, and we start the extrusion, and when we're all done, the blue resin is on the outside. It's not on the inside. How did the blue resin get to the outside? And he had a $500 contest for the students. He wanted to run a contest in MIT, see if the MIT students could do it, because out of like 50 students at this conference, only one young woman figured it out. So he was just so proud of his thing.

p51 53:09

Anyway, so does anybody have an idea how the blue resin got to the outside? Student: Diffusion? Tom: Nope, not diffusion. What have we been talking about? Inhomogeneous flow, right? Basically, if you had looked at this thing at some step in between, you would have found that you had the white sticking by friction around the boundary on the wall of the mold, and the blue bulging in front, right? So here's blue — I mean, here's white, and here's blue. Now keep doing that for a while, and the nose goes up further and further, until finally the nose folds over on itself and turns 180°. So now look at the top here. See, it folded over up there. If you had seen it at an intermediate stage, you would have seen essentially this stuff bulging — inhomogeneous flow.

p52 54:16

So he was very disappointed to find that I could solve the problem in five minutes. Now, I didn't — you — I didn't give you five minutes to solve it because we didn't have five minutes, but anyway. And we were talking earlier that it's partly because I think in terms of deforming metals, and things. Here's a polymer problem. Um, he was a chemical engineer. In his mind — and actually if you read some of the stuff, he explains this in terms of a boundary layer, that's because a chemical engineer or a mechanical engineer understands boundary layers, and they think of the world in terms of boundary layers.

p53 55:06

And I mentioned — what's your name? Mark? I mentioned Mark before most of you came to class. I had a problem once which was a problem in current flow through copper and steel when we were doing welding, and the steel would go from being ferromagnetic past the Curie temperature and stuff and become non-ferromagnetic, and so this is going to really affect the way the current flows through this thing. And so I went to see Jim Melcher, who was one of the great scientists at MIT, passed away about 15 years ago. And we started talking diffusion. And to me, diffusion is: you have a vacancy, and you have one atom move into the vacancy, and it changes places. Jim Melcher started talking diffusion, and he drew me a series of — an infinite series of parallel resistors. He thought of everything as electric circuit. I thought of diffusion in terms of atomistics. Mike Mousakas thinks in terms of the flow in Stamixco as a boundary layer problem. I think of it as inhomogeneous deformation, okay. So even though we're all engineers, we speak different languages. That's one of the lessons for today, okay. I'll see you on, um, Tuesday.